Technology Process of 1-(4-hexadecylphenyl)-3-phenylpropan-2-one
There total 8 articles about 1-(4-hexadecylphenyl)-3-phenylpropan-2-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 30 percent / triethylsilane; trifluoroacetic acid / 20 °C
2.1: isopropylmagnesium chloride / tetrahydrofuran / 20 h / Heating
2.2: 37 percent / tetrahydrofuran / cooling
3.1: 70 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating
4.1: tetrabutylammonium fluoride / acetonitrile / 2 h
5.1: sodium ethoxide / ethanol; heptane / 20 h / Heating
6.1: 1.5 g / aq. H2SO4 / 48 h / Heating
With
triethylsilane; lithium aluminium tetrahydride; sulfuric acid; tetrabutyl ammonium fluoride; isopropylmagnesium chloride; sodium ethanolate; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; n-heptane; acetonitrile;
DOI:10.1021/ja067461q
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutylammonium fluoride / acetonitrile / 2 h
2: sodium ethoxide / ethanol; heptane / 20 h / Heating
3: 1.5 g / aq. H2SO4 / 48 h / Heating
With
sulfuric acid; tetrabutyl ammonium fluoride; sodium ethanolate;
In
ethanol; n-heptane; acetonitrile;
DOI:10.1021/ja067461q
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium ethoxide / ethanol; heptane / 20 h / Heating
2: 1.5 g / aq. H2SO4 / 48 h / Heating
With
sulfuric acid; sodium ethanolate;
In
ethanol; n-heptane;
DOI:10.1021/ja067461q
