(4-hexadecylphenyl)methanol

Base Information

Chemical Name:(4-hexadecylphenyl)methanol
CAS No.:936574-71-9
Molecular Formula:C₂₃H₄₀O
Molecular Weight:332.57
Hs Code.:

Synonyms:(4-hexadecylphenyl)methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-hexadecylphenyl)methanol

Chemical Property:

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Technology Process of (4-hexadecylphenyl)methanol

There total 5 articles about (4-hexadecylphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 23812-34-2
4-hexadecylbenzoic acid

: 936574-71-9
(4-hexadecylphenyl)methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 24h; Heating;
DOI:10.1021/ja067461q

Reference yield:

: 116526-71-7
1-(4-bromophenyl)hexadecan-1-one

: 936574-71-9
(4-hexadecylphenyl)methanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 30 percent / triethylsilane; trifluoroacetic acid / 20 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 20 h / Heating

2.2: 37 percent / tetrahydrofuran / cooling

3.1: 70 percent / LiAlH₄ / tetrahydrofuran / 24 h / Heating

With triethylsilane; lithium aluminium tetrahydride; isopropylmagnesium chloride; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/ja067461q

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 936574-71-9
(4-hexadecylphenyl)methanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 34 percent / AlCl₃ / 1 h / 70 °C

2.1: 30 percent / triethylsilane; trifluoroacetic acid / 20 °C

3.1: isopropylmagnesium chloride / tetrahydrofuran / 20 h / Heating

3.2: 37 percent / tetrahydrofuran / cooling

4.1: 70 percent / LiAlH₄ / tetrahydrofuran / 24 h / Heating

With triethylsilane; lithium aluminium tetrahydride; aluminium trichloride; isopropylmagnesium chloride; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/ja067461q