(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di-(benzoyloxy)-1,1-diethylthio-5-iodohexane

Base Information

Chemical Name:(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di-(benzoyloxy)-1,1-diethylthio-5-iodohexane
CAS No.:358395-60-5
Molecular Formula:C₄₀H₄₇IO₅S₂Si
Molecular Weight:826.932
Hs Code.:

Synonyms:(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di-(benzoyloxy)-1,1-diethylthio-5-iodohexane

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Chemical Property of (2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di-(benzoyloxy)-1,1-diethylthio-5-iodohexane

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Technology Process of (2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di-(benzoyloxy)-1,1-diethylthio-5-iodohexane

There total 2 articles about (2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di-(benzoyloxy)-1,1-diethylthio-5-iodohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 98-88-4
benzoyl chloride

: 358395-59-2
(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-1,1-diethylthio-5-iodohexane-2,4-diol

: 358395-60-5
(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di-(benzoyloxy)-1,1-diethylthio-5-iodohexane

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1016/S0040-4039(01)00754-7

Reference yield:

: tert-Butyl-[(R)-2-((3aS,5R,6aS)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-iodo-ethoxy]-diphenyl-silane

: 358395-60-5
(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di-(benzoyloxy)-1,1-diethylthio-5-iodohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / ZnCl₂ / 0.5 h / -20 °C

2: 88 percent / pyridine / 20 °C

With zinc(II) chloride; In pyridine;
DOI:10.1016/S0040-4020(03)00258-8