(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di(benzoyloxy)-5-iodohexanal

Base Information

Chemical Name:(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di(benzoyloxy)-5-iodohexanal
CAS No.:358395-61-6
Molecular Formula:C₃₆H₃₇IO₆Si
Molecular Weight:720.676
Hs Code.:

Synonyms:(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di(benzoyloxy)-5-iodohexanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di(benzoyloxy)-5-iodohexanal

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Technology Process of (2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di(benzoyloxy)-5-iodohexanal

There total 5 articles about (2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di(benzoyloxy)-5-iodohexanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 358395-60-5
(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di-(benzoyloxy)-1,1-diethylthio-5-iodohexane

: 358395-61-6
(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di(benzoyloxy)-5-iodohexanal

Guidance literature:: With mercury dichloride; mercury(II) oxide; In water; acetone;
DOI:10.1016/S0040-4039(01)00754-7

Reference yield:

: tert-Butyl-[(R)-2-((3aS,5R,6aS)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-iodo-ethoxy]-diphenyl-silane

: 358395-61-6
(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di(benzoyloxy)-5-iodohexanal

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / ZnCl₂ / 0.5 h / -20 °C

2: 88 percent / pyridine / 20 °C

3: 100 percent / HgO; HgCl₂ / acetone; H₂O / Heating

With mercury dichloride; mercury(II) oxide; zinc(II) chloride; In pyridine; water; acetone;
DOI:10.1016/S0040-4020(03)00258-8

Reference yield:

: 358395-59-2
(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-1,1-diethylthio-5-iodohexane-2,4-diol

: 358395-61-6
(2S,4R,5R)-6-(tert-butyldiphenylsilyloxy)-2,4-di(benzoyloxy)-5-iodohexanal

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / pyridine / 20 °C

2: 100 percent / HgO; HgCl₂ / acetone; H₂O / Heating

With mercury dichloride; mercury(II) oxide; In pyridine; water; acetone;
DOI:10.1016/S0040-4020(03)00258-8