methyl 4-(t-butoxycarbonyl(3-methoxy-3-oxo-2-phenylpropyl)amino)butanoate

Base Information

Chemical Name:methyl 4-(t-butoxycarbonyl(3-methoxy-3-oxo-2-phenylpropyl)amino)butanoate
CAS No.:1356654-18-6
Molecular Formula:C₂₀H₂₉NO₆
Molecular Weight:379.453
Hs Code.:

Synonyms:methyl 4-(t-butoxycarbonyl(3-methoxy-3-oxo-2-phenylpropyl)amino)butanoate

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Chemical Property of methyl 4-(t-butoxycarbonyl(3-methoxy-3-oxo-2-phenylpropyl)amino)butanoate

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Technology Process of methyl 4-(t-butoxycarbonyl(3-methoxy-3-oxo-2-phenylpropyl)amino)butanoate

There total 4 articles about methyl 4-(t-butoxycarbonyl(3-methoxy-3-oxo-2-phenylpropyl)amino)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1356654-17-5
methyl 4-(benzyl(3-methoxy-3-oxo-2-phenylpropyl)amino)butanoate

: 1356654-18-6
methyl 4-(t-butoxycarbonyl(3-methoxy-3-oxo-2-phenylpropyl)amino)butanoate

Guidance literature:: With hydrogen; palladium(II) hydroxide; In ethanol; at 20 ℃; for 16h; under 2068.65 Torr; Autoclave;
DOI:10.1016/j.tetlet.2011.11.129

Reference yield:

: 101584-49-0
methyl 3-(benzylamino)-2-phenylpropanoate

: 1356654-18-6
methyl 4-(t-butoxycarbonyl(3-methoxy-3-oxo-2-phenylpropyl)amino)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / 1,4-dioxane; water / 64 h / 100 °C

2: hydrogen; palladium(II) hydroxide / ethanol / 16 h / 20 °C / 2068.65 Torr / Autoclave

With hydrogen; palladium(II) hydroxide; potassium carbonate; potassium iodide; In 1,4-dioxane; ethanol; water;
DOI:10.1016/j.tetlet.2011.11.129

Reference yield:

: 1865-29-8
2-phenyl-acrylic acid methyl ester

: 1356654-18-6
methyl 4-(t-butoxycarbonyl(3-methoxy-3-oxo-2-phenylpropyl)amino)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 18 h / 20 °C

2: potassium carbonate; potassium iodide / 1,4-dioxane; water / 64 h / 100 °C

3: hydrogen; palladium(II) hydroxide / ethanol / 16 h / 20 °C / 2068.65 Torr / Autoclave

With hydrogen; palladium(II) hydroxide; potassium carbonate; potassium iodide; In 1,4-dioxane; methanol; ethanol; water;
DOI:10.1016/j.tetlet.2011.11.129