benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside
CAS No.:1338712-04-1
Molecular Formula:C₃₉H₃₃NO₁₀S
Molecular Weight:707.758
Hs Code.:

Synonyms:benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside

Suppliers and Price of benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside

There total 1 articles about benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 862537-77-7
benzoxazol-2-yl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: 591-80-0
pent-4-enoic acid

: 1338712-04-1
benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In 1,2-dichloro-ethane; at 0 - 40 ℃; for 17h;
DOI:10.1039/c1cc13409d

Reference yield: 85.0%

: 142719-06-0
methyl 2,3,4-tri-O-benzyl-6-O-(4-methoxybenzyl)-α-D-glucopyranoside

: 1338712-04-1
benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside

: 1338712-10-9
methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-pentenoyl-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: methyl 2,3,4-tri-O-benzyl-6-O-(4-methoxybenzyl)-α-D-glucopyranoside; benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside; With 1-(Trimethylsilyl)imidazole; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 0.5h; Molecular sieve; Darkness;

With silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 20 ℃; for 2h; Molecular sieve;
DOI:10.1039/c1cc13409d

Reference yield: 82.0%

: 1338712-04-1
benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside

: 1338712-09-6
methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside

: 1338712-11-0
methyl 2,3,4-tri-O-benzyl-6-O-[2,3,4-tri-O-benzoyl-6-O-(2,3,4-tri-O-benzoyl-6-Opentenoyl-α-D-glucopyranosyl)-α-D-glucopyranosyl]-β-D-glucopyranoside

Guidance literature:: benzoxazolyl 2,3,4-tri-O-benzoyl-6-O-pentenoyl-1-thio-β-D-glucopyranoside; methyl 2,3,4-tri-O-benzyl-6-O-(2,3,4-tri-O-benzoyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-α-D-glucopyranoside; With 1-(Trimethylsilyl)imidazole; In 1,2-dichloro-ethane; at 0 ℃; for 0.5h; Molecular sieve; Darkness;

With silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 40 ℃; for 2h; Molecular sieve;
DOI:10.1039/c1cc13409d