5-Methoxy-4-methyl-2-(phenylmethoxy)benzaldehyde

Base Information

Chemical Name:5-Methoxy-4-methyl-2-(phenylmethoxy)benzaldehyde
CAS No.:74516-55-5
Molecular Formula:C₁₆H₁₆O₃
Molecular Weight:256.301
Hs Code.:
DSSTox Substance ID:DTXSID501236887

Synonyms:5-Methoxy-4-methyl-2-(phenylmethoxy)benzaldehyde;DTXSID501236887;74516-55-5

Suppliers and Price of 5-Methoxy-4-methyl-2-(phenylmethoxy)benzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Methoxy-4-methyl-2-(phenylmethoxy)benzaldehyde

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:256.109944368
Heavy Atom Count:19
Complexity:273

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=C(C=C1OC)C=O)OCC2=CC=CC=C2

Technology Process of 5-Methoxy-4-methyl-2-(phenylmethoxy)benzaldehyde

There total 2 articles about 5-Methoxy-4-methyl-2-(phenylmethoxy)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 100-39-0
benzyl bromide

: 74516-54-4
2-hydroxy-4-methyl-5-methoxybenzaldehyde

: 74516-55-5
2-(benzyloxy)-4-methyl-5-methoxybezaldehyde

Guidance literature:: With potassium carbonate; In ethanol; for 16h; Heating;
DOI:10.1021/jm00183a006

Reference yield:

: 4925-88-6
2,5-dimethoxy-4-methylbenzaldehyde

: 74516-55-5
2-(benzyloxy)-4-methyl-5-methoxybezaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / BCl₃ / CH₂Cl₂ / -78 - 20 °C

2: 49 percent / K₂CO₃ / aq. ethanol / 16 h / Heating

With boron trichloride; potassium carbonate; In ethanol; dichloromethane;
DOI:10.1021/jm00183a006