(3S,4R)-3,5-dibenzyloxy-1-bromo-4-formyloxy-1,1,2,2-tetrafluoropentane

Base Information

Chemical Name:(3S,4R)-3,5-dibenzyloxy-1-bromo-4-formyloxy-1,1,2,2-tetrafluoropentane
CAS No.:1050610-64-4
Molecular Formula:C₂₀H₁₉BrF₄O₄
Molecular Weight:479.266
Hs Code.:

Synonyms:(3S,4R)-3,5-dibenzyloxy-1-bromo-4-formyloxy-1,1,2,2-tetrafluoropentane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4R)-3,5-dibenzyloxy-1-bromo-4-formyloxy-1,1,2,2-tetrafluoropentane

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Technology Process of (3S,4R)-3,5-dibenzyloxy-1-bromo-4-formyloxy-1,1,2,2-tetrafluoropentane

There total 2 articles about (3S,4R)-3,5-dibenzyloxy-1-bromo-4-formyloxy-1,1,2,2-tetrafluoropentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 64-18-6
formic acid

: 1050610-60-0
(3S,4R)-3,5-bisbenzyloxy1-bromo-1,1,2,2-tetrafluoropentane-4-ol

: 1050610-64-4
(3S,4R)-3,5-dibenzyloxy-1-bromo-4-formyloxy-1,1,2,2-tetrafluoropentane

Guidance literature:: With dmap; diisopropyl-carbodiimide; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol801272e

Reference yield: 92.0%

: 1050610-60-0
(3S,4R)-3,5-bisbenzyloxy1-bromo-1,1,2,2-tetrafluoropentane-4-ol

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1050610-64-4
(3S,4R)-3,5-dibenzyloxy-1-bromo-4-formyloxy-1,1,2,2-tetrafluoropentane

Guidance literature:: With pyridine; p-toluenesulfonyl chloride; at 0 - 20 ℃; for 1.5h;
DOI:10.1021/acs.joc.6b00302

Reference yield: 81.0%

: 1050610-64-4
(3S,4R)-3,5-dibenzyloxy-1-bromo-4-formyloxy-1,1,2,2-tetrafluoropentane

: 4,6-di-O-benzyl-2,3-dideoxy-2,2,3,3-tetrafluoro-threo-hexopyranose

Guidance literature:: With methyllithium; In tetrahydrofuran; diethyl ether; at -78 ℃; for 4.5h; Inert atmosphere;
DOI:10.1021/acs.joc.6b00302