(4-methoxy-phenyl)-2-thio-oxalomonoimidic acid-2-amide-1-p-anisidide

Base Information

• Chemical Name: (4-methoxy-phenyl)-2-thio-oxalomonoimidic acid-2-amide-1-p-anisidide
• CAS No.: 858798-69-3
• Molecular Formula: C₁₆H₁₇N₃O₂S
• Molecular Weight: 315.396
• Mol file: 858798-69-3.mol

Synonyms:(4-methoxy-phenyl)-2-thio-oxalomonoimidic acid-2-amide-1-p-anisidide

Chemical Property of (4-methoxy-phenyl)-2-thio-oxalomonoimidic acid-2-amide-1-p-anisidide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (4-methoxy-phenyl)-2-thio-oxalomonoimidic acid-2-amide-1-p-anisidide

There total 3 articles about (4-methoxy-phenyl)-2-thio-oxalomonoimidic acid-2-amide-1-p-anisidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile (640732-63-4) → (4-methoxy-phenyl)-2-thio-oxalomonoimidic acid-2-amide-1-p-anisidide (858798-69-3)

Guidance literature:

With ammonium polysulfide; at 45 ℃;

Reference yield:

4-methoxy-aniline (104-94-9) → (4-methoxy-phenyl)-2-thio-oxalomonoimidic acid-2-amide-1-p-anisidide (858798-69-3)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanolic KOH-solution

2: basic lead carbonate; aqueous ethanol / 50 - 60 °C

3: aqueous ammonium polysulfide / 45 °C

With potassium hydroxide; ammonium polysulfide; ethanol; basic lead(II) carbonate;

Reference yield:

1,3-bis-(p-methoxyphenyl)thiourea (1227-45-8) → (4-methoxy-phenyl)-2-thio-oxalomonoimidic acid-2-amide-1-p-anisidide (858798-69-3)

Guidance literature:

Multi-step reaction with 2 steps

1: basic lead carbonate; aqueous ethanol / 50 - 60 °C

2: aqueous ammonium polysulfide / 45 °C

With ammonium polysulfide; ethanol; basic lead(II) carbonate;

upstream raw materials:

(4-methoxy-phenyl)-oxalomonoimidic acid p-anisidide-nitrile

4-methoxy-aniline

1,3-bis-(p-methoxyphenyl)thiourea

Downstream raw materials:

5-methoxyisatine