ethyl (R/S)-2--3,3-diethoxypropionate

Base Information

Chemical Name:ethyl (R/S)-2--3,3-diethoxypropionate
CAS No.:134936-25-7
Molecular Formula:C₂₅H₃₃NO₆
Molecular Weight:443.54
Hs Code.:

ethyl (R/S)-2-<benzoyl(2-benzyloxyethyl)amino>-3,3-diethoxypropionate

Synonyms:ethyl (R/S)-2--3,3-diethoxypropionate

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Chemical Property of ethyl (R/S)-2--3,3-diethoxypropionate

Chemical Property:

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Technology Process of ethyl (R/S)-2--3,3-diethoxypropionate

There total 7 articles about ethyl (R/S)-2--3,3-diethoxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 134936-24-6
ethyl (R/S)-2-<(benzyloxyethyl)amino>-3,3-diethoxypropionate

: 98-88-4
benzoyl chloride

: 134936-25-7
ethyl (R/S)-2--3,3-diethoxypropionate

Guidance literature:: With pyridine; In dichloromethane; for 3h;

Reference yield:

: 134936-21-3
ethyl (R/S)-2-(dibenzylamino)-3-hydroxy-2-propenoate

: 134936-25-7
ethyl (R/S)-2--3,3-diethoxypropionate

Guidance literature:: Multi-step reaction with 4 steps

1: conc. sulfuric acid / ethanol / 2 h / Heating

2: 95 percent / H₂, acetic acid / palladium(II) hydroxide/carbon (20percent) / aq. ethanol / 3 h / 3000.2 Torr / Ambient temperature

3: 64 percent / sodium cyanoborohydride / methanol / 16 h

4: 78 percent / pyridine / CH₂Cl₂ / 3 h

With pyridine; sulfuric acid; hydrogen; sodium cyanoborohydride; acetic acid; palladium dihydroxide; pyrographite; In methanol; ethanol; dichloromethane;

Reference yield:

: 134936-23-5
ethyl (R/S)-2-(dibenzylamino)-3,3-diethoxypropionate

: 134936-25-7
ethyl (R/S)-2--3,3-diethoxypropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂, acetic acid / palladium(II) hydroxide/carbon (20percent) / aq. ethanol / 3 h / 3000.2 Torr / Ambient temperature

2: 64 percent / sodium cyanoborohydride / methanol / 16 h

3: 78 percent / pyridine / CH₂Cl₂ / 3 h

With pyridine; hydrogen; sodium cyanoborohydride; acetic acid; palladium dihydroxide; pyrographite; In methanol; ethanol; dichloromethane;