{2-[4-(2-Benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid monodecyl ester

Base Information

Chemical Name:{2-[4-(2-Benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid monodecyl ester
CAS No.:287970-42-7
Molecular Formula:C₃₃H₅₃O₇P
Molecular Weight:592.753
Hs Code.:

Synonyms:{2-[4-(2-Benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid monodecyl ester

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Chemical Property of {2-[4-(2-Benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid monodecyl ester

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Technology Process of {2-[4-(2-Benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid monodecyl ester

There total 14 articles about {2-[4-(2-Benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid monodecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 287970-39-2
{2-[4-(2-benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid didecyl ester

: 287970-42-7
{2-[4-(2-Benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid monodecyl ester

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; water; Heating;
DOI:10.1016/S0040-4039(00)00438-X

Reference yield:

: 622-08-2,1201808-31-2
2-Benzyloxyethanol

: 287970-42-7
{2-[4-(2-Benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid monodecyl ester

Guidance literature:: Multi-step reaction with 11 steps

1.1: NaH / dimethylformamide

2.1: NMO / OsO₄ / acetone; H₂O

3.1: Bu₂SnO / toluene / Heating

3.2: n-Bu₄NI

4.1: NaH / dimethylformamide

5.1: NMO / OsO₄ / acetone; H₂O

6.1: Na₂SO₃; NaIO₄

7.1: NaBH₄ / ethanol

8.1: Et₃N / CH₂Cl₂

9.1: n-Bu₄NBr / toluene / Heating

10.1: 73 percent / 170 °C

11.1: 56 percent / NaOH / dioxane; H₂O / Heating

With sodium hydroxide; sodium tetrahydroborate; sodium periodate; N-methyl-2-indolinone; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; triethylamine; sodium sulfite; osmium(VIII) oxide; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; 1.1: Alkylation / 2.1: Hydroxylation / 3.1: Stannylation / 3.2: Benzylation / 4.1: Allylation / 5.1: Hydroxylation / 6.1: Diol cleavage / 7.1: Reduction / 8.1: Mesylation / 9.1: Bromination / 10.1: Substitution / 11.1: Hydrolysis;
DOI:10.1016/S0040-4039(00)00438-X

Reference yield:

: 100-39-0
benzyl bromide

: 287970-42-7
{2-[4-(2-Benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid monodecyl ester

Guidance literature:: Multi-step reaction with 9 steps

1.1: Bu₂SnO / toluene / Heating

1.2: n-Bu₄NI

2.1: NaH / dimethylformamide

3.1: NMO / OsO₄ / acetone; H₂O

4.1: Na₂SO₃; NaIO₄

5.1: NaBH₄ / ethanol

6.1: Et₃N / CH₂Cl₂

7.1: n-Bu₄NBr / toluene / Heating

8.1: 73 percent / 170 °C

9.1: 56 percent / NaOH / dioxane; H₂O / Heating

With sodium hydroxide; sodium tetrahydroborate; sodium periodate; N-methyl-2-indolinone; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; triethylamine; sodium sulfite; osmium(VIII) oxide; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; 1.1: Stannylation / 1.2: Benzylation / 2.1: Allylation / 3.1: Hydroxylation / 4.1: Diol cleavage / 5.1: Reduction / 6.1: Mesylation / 7.1: Bromination / 8.1: Substitution / 9.1: Hydrolysis;
DOI:10.1016/S0040-4039(00)00438-X