{2-[4-(2-benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid didecyl ester

Base Information

Chemical Name:{2-[4-(2-benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid didecyl ester
CAS No.:287970-39-2
Molecular Formula:C₄₃H₇₃O₇P
Molecular Weight:733.022
Hs Code.:

Synonyms:{2-[4-(2-benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid didecyl ester

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Chemical Property of {2-[4-(2-benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid didecyl ester

Chemical Property:

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Technology Process of {2-[4-(2-benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid didecyl ester

There total 12 articles about {2-[4-(2-benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid didecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 2929-86-4,15836-55-2
tridecyl phosphite

: 287970-37-0
C₂₃H₃₁BrO₄

: 287970-39-2
{2-[4-(2-benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid didecyl ester

Guidance literature:: at 170 ℃;
DOI:10.1016/S0040-4039(00)00438-X

Reference yield:

: 622-08-2,1201808-31-2
2-Benzyloxyethanol

: 287970-39-2
{2-[4-(2-benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid didecyl ester

Guidance literature:: Multi-step reaction with 10 steps

1.1: NaH / dimethylformamide

2.1: NMO / OsO₄ / acetone; H₂O

3.1: Bu₂SnO / toluene / Heating

3.2: n-Bu₄NI

4.1: NaH / dimethylformamide

5.1: NMO / OsO₄ / acetone; H₂O

6.1: Na₂SO₃; NaIO₄

7.1: NaBH₄ / ethanol

8.1: Et₃N / CH₂Cl₂

9.1: n-Bu₄NBr / toluene / Heating

10.1: 73 percent / 170 °C

With sodium tetrahydroborate; sodium periodate; N-methyl-2-indolinone; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; triethylamine; sodium sulfite; osmium(VIII) oxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; 1.1: Alkylation / 2.1: Hydroxylation / 3.1: Stannylation / 3.2: Benzylation / 4.1: Allylation / 5.1: Hydroxylation / 6.1: Diol cleavage / 7.1: Reduction / 8.1: Mesylation / 9.1: Bromination / 10.1: Substitution;
DOI:10.1016/S0040-4039(00)00438-X

Reference yield:

: 100-39-0
benzyl bromide

: 287970-39-2
{2-[4-(2-benzyloxy-ethoxy)-1-benzyloxymethyl-butoxy]-ethyl}-phosphonic acid didecyl ester

Guidance literature:: Multi-step reaction with 8 steps

1.1: Bu₂SnO / toluene / Heating

1.2: n-Bu₄NI

2.1: NaH / dimethylformamide

3.1: NMO / OsO₄ / acetone; H₂O

4.1: Na₂SO₃; NaIO₄

5.1: NaBH₄ / ethanol

6.1: Et₃N / CH₂Cl₂

7.1: n-Bu₄NBr / toluene / Heating

8.1: 73 percent / 170 °C

With sodium tetrahydroborate; sodium periodate; N-methyl-2-indolinone; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; triethylamine; sodium sulfite; osmium(VIII) oxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; 1.1: Stannylation / 1.2: Benzylation / 2.1: Allylation / 3.1: Hydroxylation / 4.1: Diol cleavage / 5.1: Reduction / 6.1: Mesylation / 7.1: Bromination / 8.1: Substitution;
DOI:10.1016/S0040-4039(00)00438-X