N,N-di-n-propyl-(p-chlorophenylthio)-(1-benzenesulfonyl-6-benzenesulfonyloxy-5-indolinyl)-acetamide

Base Information

Chemical Name:N,N-di-n-propyl-(p-chlorophenylthio)-(1-benzenesulfonyl-6-benzenesulfonyloxy-5-indolinyl)-acetamide
CAS No.:155636-51-4
Molecular Formula:C₃₄H₃₅ClN₂O₆S₃
Molecular Weight:699.313
Hs Code.:

Synonyms:N,N-di-n-propyl-(p-chlorophenylthio)-(1-benzenesulfonyl-6-benzenesulfonyloxy-5-indolinyl)-acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-di-n-propyl-(p-chlorophenylthio)-(1-benzenesulfonyl-6-benzenesulfonyloxy-5-indolinyl)-acetamide

Chemical Property:

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Technology Process of N,N-di-n-propyl-(p-chlorophenylthio)-(1-benzenesulfonyl-6-benzenesulfonyloxy-5-indolinyl)-acetamide

There total 6 articles about N,N-di-n-propyl-(p-chlorophenylthio)-(1-benzenesulfonyl-6-benzenesulfonyloxy-5-indolinyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2042-14-0
4-methyl-5-nitrophenol

: 155636-51-4
N,N-di-n-propyl-(p-chlorophenylthio)-(1-benzenesulfonyl-6-benzenesulfonyloxy-5-indolinyl)-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / K₂CO₃ / acetone / 2 h

2: 2.) TiCl₃, ammonium acetate / 1.) DMF, 120 deg C, 5 h, 2.) MeOH, 10 min

3: NaBH₃CN, acetic acid / 4 h / Ambient temperature

4: Et₃N / acetic acid / 1 h

5: 1.) TFAA, 2.) SnCl₄ / 1.) CH₂Cl₂, 20 min, 2.) CH₂Cl₂, RT, overnight

With ammonium acetate; titanium(III) chloride; tin(IV) chloride; sodium cyanoborohydride; potassium carbonate; acetic acid; triethylamine; trifluoroacetic anhydride; In acetic acid; acetone;
DOI:10.1080/00397919408011708

Reference yield:

: 92059-54-6
4-benzenesulfonyloxy-2-nitrotoluene

: 155636-51-4
N,N-di-n-propyl-(p-chlorophenylthio)-(1-benzenesulfonyl-6-benzenesulfonyloxy-5-indolinyl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) TiCl₃, ammonium acetate / 1.) DMF, 120 deg C, 5 h, 2.) MeOH, 10 min

2: NaBH₃CN, acetic acid / 4 h / Ambient temperature

3: Et₃N / acetic acid / 1 h

4: 1.) TFAA, 2.) SnCl₄ / 1.) CH₂Cl₂, 20 min, 2.) CH₂Cl₂, RT, overnight

With ammonium acetate; titanium(III) chloride; tin(IV) chloride; sodium cyanoborohydride; acetic acid; triethylamine; trifluoroacetic anhydride; In acetic acid;
DOI:10.1080/00397919408011708

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 155636-51-4
N,N-di-n-propyl-(p-chlorophenylthio)-(1-benzenesulfonyl-6-benzenesulfonyloxy-5-indolinyl)-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / K₂CO₃ / acetone / 2 h

2: 2.) TiCl₃, ammonium acetate / 1.) DMF, 120 deg C, 5 h, 2.) MeOH, 10 min

3: NaBH₃CN, acetic acid / 4 h / Ambient temperature

4: Et₃N / acetic acid / 1 h

5: 1.) TFAA, 2.) SnCl₄ / 1.) CH₂Cl₂, 20 min, 2.) CH₂Cl₂, RT, overnight

With ammonium acetate; titanium(III) chloride; tin(IV) chloride; sodium cyanoborohydride; potassium carbonate; acetic acid; triethylamine; trifluoroacetic anhydride; In acetic acid; acetone;
DOI:10.1080/00397919408011708