trimethyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-quaternaryammonium bromide

Base Information

Chemical Name:trimethyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-quaternaryammonium bromide
CAS No.:1447933-45-0
Molecular Formula:Br*C₁₆H₂₇BNO₂
Molecular Weight:356.111
Hs Code.:

Synonyms:trimethyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-quaternaryammonium bromide

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Chemical Property of trimethyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-quaternaryammonium bromide

Chemical Property:

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Technology Process of trimethyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-quaternaryammonium bromide

There total 14 articles about trimethyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-quaternaryammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73183-34-3
bis(pinacol)diborane

: 1447933-45-0
trimethyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-quaternaryammonium bromide

Guidance literature:: Multi-step reaction with 6 steps

1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 48 h / 85 °C / Inert atmosphere

2: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / acetonitrile / 2 h / 90 °C / Inert atmosphere

3: dihydrogen peroxide; water / 20 °C

4: toluene / 2 h / Reflux

5: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / acetonitrile / 2 h / 90 °C / Inert atmosphere

6: acetonitrile; ethanol / 12 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); water; dihydrogen peroxide; potassium acetate; In ethanol; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/chem.201300539

Reference yield:

: 883715-40-0
2-(2-methyl-4-nitrophenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1447933-45-0
trimethyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-quaternaryammonium bromide

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / acetonitrile / 2 h / 90 °C / Inert atmosphere

2: dihydrogen peroxide; water / 20 °C

3: toluene / 2 h / Reflux

4: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / acetonitrile / 2 h / 90 °C / Inert atmosphere

5: acetonitrile; ethanol / 12 h / 20 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); water; dihydrogen peroxide; In ethanol; toluene; acetonitrile;
DOI:10.1002/chem.201300539

Reference yield:

: 214360-64-2
2-(2,4-bismethylphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1447933-45-0
trimethyl-[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl]-quaternaryammonium bromide

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / acetonitrile / 2 h / 90 °C / Inert atmosphere

2: dihydrogen peroxide; water / 20 °C

3: toluene / 2 h / Reflux

4: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / acetonitrile / 2 h / 90 °C / Inert atmosphere

5: acetonitrile; ethanol / 12 h / 20 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); water; dihydrogen peroxide; In ethanol; toluene; acetonitrile;
DOI:10.1002/chem.201300539