C₁₄H₁₆ClNO₃

Base Information

Chemical Name:C₁₄H₁₆ClNO₃
CAS No.:1541198-24-6
Molecular Formula:C₁₄H₁₆ClNO₃
Molecular Weight:281.739
Hs Code.:

C<sub>14</sub>H<sub>16</sub>ClNO<sub>3</sub>

Synonyms:C₁₄H₁₆ClNO₃

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Chemical Property of C₁₄H₁₆ClNO₃

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Technology Process of C₁₄H₁₆ClNO₃

There total 7 articles about C₁₄H₁₆ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1541198-23-5
C₁₄H₁₅ClO₄

: 1541198-24-6
C₁₄H₁₆ClNO₃

Guidance literature:: With tert-butyl chloroformate; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 3721-95-7
Cyclobutanecarboxylic acid

: 1541198-24-6
C₁₄H₁₆ClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 8 h / 70 °C

2.1: n-butyllithium; N-cyclohexyl-cyclohexanamine / hexane; toluene / 0.25 h / 0 - 25 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: water; sodium hydroxide / methanol / 3 h / 80 °C

4.1: tert-butyl chloroformate; triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With n-butyllithium; sulfuric acid; water; tert-butyl chloroformate; triethylamine; N-cyclohexyl-cyclohexanamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; toluene;

Reference yield:

: 765-85-5
methyl cyclobutanecarboxylate

: 1541198-24-6
C₁₄H₁₆ClNO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; N-cyclohexyl-cyclohexanamine / hexane; toluene / 0.25 h / 0 - 25 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: water; sodium hydroxide / methanol / 3 h / 80 °C

3.1: tert-butyl chloroformate; triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With n-butyllithium; water; tert-butyl chloroformate; triethylamine; N-cyclohexyl-cyclohexanamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; toluene;