1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane

Base Information

Chemical Name:1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane
CAS No.:959411-85-9
Molecular Formula:C₃₄H₃₆N₂O₄
Molecular Weight:536.671
Hs Code.:

Synonyms:1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane

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Chemical Property of 1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane

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Technology Process of 1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane

There total 1 articles about 1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 629-03-8
1 ,6-dibromohexane

: 20919-36-2
N-benzylsalicylamide

: 959411-85-9
1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 - 85 ℃; for 15h;
DOI:10.1016/j.saa.2006.12.060

Reference yield: 80.0%

: 959411-85-9
1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane

: terbium(III) nitrate hexahydrate

: 2Tb(NO₃)3*3(1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane)*4H₂O

Guidance literature:: In chloroform; ethyl acetate; soln. Ln(NO3)3*6H2O in EtOAc was added dropwise to soln. ligand in CHCl3and stirred at room temp. for 4 h; ppt. was filtered, washed with EtOAc and CHCl3 and dried in vacuo over P2O5; elem. anal.;
DOI:10.1016/j.saa.2006.12.060

Reference yield: 80.0%

: 959411-85-9
1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane

: europium(III) nitrate hexahydrate

: 2Eu(NO₃)3*3(1,6-bis[(2'-benzylaminoformyl)phenoxyl]hexane)*4H₂O

Guidance literature:: In chloroform; ethyl acetate; 2 equiv. of EtOAc soln. of metal salt was added to 3 equiv. of CHCl3 soln. of phenoxy-compd., stirring at room temp. for 4 h; solid was filtered off, washed with EtOAc and CHCl3, dried in vac. over P4O10 for 48 h, elem. anal.;
DOI:10.1016/j.inoche.2007.03.025