2-Chloro-3-(β-ethylamino-β-methyl-α-ethoxycarbonyl)vinyl-5-methylhydroquinone

Base Information

• Chemical Name: 2-Chloro-3-(β-ethylamino-β-methyl-α-ethoxycarbonyl)vinyl-5-methylhydroquinone
• CAS No.: 129247-34-3
• Molecular Formula: C₁₅H₂₀ClNO₄
• Molecular Weight: 313.781

Synonyms:2-Chloro-3-(β-ethylamino-β-methyl-α-ethoxycarbonyl)vinyl-5-methylhydroquinone

Chemical Property of 2-Chloro-3-(β-ethylamino-β-methyl-α-ethoxycarbonyl)vinyl-5-methylhydroquinone

Chemical Property:

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Technology Process of 2-Chloro-3-(β-ethylamino-β-methyl-α-ethoxycarbonyl)vinyl-5-methylhydroquinone

There total 1 articles about 2-Chloro-3-(β-ethylamino-β-methyl-α-ethoxycarbonyl)vinyl-5-methylhydroquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

2-chloro-5-methyl-1,4-benzoquinone (19832-87-2) + ethyl 3-ethylamino-2-butenoate (13070-53-6) → 1-Ethyl-2,7-dimethyl-3-ethoxycarbonyl-4-chloro-5-hydroxyindole (129247-32-1) + 2-Chloro-3-(β-ethylamino-β-methyl-α-ethoxycarbonyl)vinyl-5-methylhydroquinone (129247-34-3)

Guidance literature:

In methanol; at -5 ℃;

DOI:10.1007/BF00472542

Reference yield: 90.0%

2-Chloro-3-(β-ethylamino-β-methyl-α-ethoxycarbonyl)vinyl-5-methylhydroquinone (129247-34-3) → 2-Chloro-3-(β-ethylamino-β-methyl-α-ethoxycabonl)vinyl-5-methylbenzoquinone (129247-36-5)

Guidance literature:

With silver(l) oxide; In diethyl ether;

DOI:10.1007/BF00472542

upstream raw materials:

2-chloro-5-methyl-1,4-benzoquinone

ethyl 3-ethylamino-2-butenoate

Downstream raw materials:

2-Chloro-3-(β-ethylamino-β-methyl-α-ethoxycabonl)vinyl-5-methylbenzoquinone

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