1-(N-β-D-galactopyranosyl)-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

Base Information

Chemical Name:1-(N-β-D-galactopyranosyl)-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole
CAS No.:1467042-79-0
Molecular Formula:C₂₇H₂₉N₃O₁₁
Molecular Weight:571.541
Hs Code.:

Synonyms:1-(N-β-D-galactopyranosyl)-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

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Chemical Property of 1-(N-β-D-galactopyranosyl)-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

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Technology Process of 1-(N-β-D-galactopyranosyl)-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

There total 3 articles about 1-(N-β-D-galactopyranosyl)-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1467042-70-1
1-[N-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)]-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

: 1467042-79-0
1-(N-β-D-galactopyranosyl)-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

Guidance literature:: With methanol; sodium methylate; at 20 ℃; for 4h;
DOI:10.2174/15701786113109990039

Reference yield:

: 1467042-67-6
5,7-dimethoxy-2-(4-methoxyphenyl)-3-(prop-2-yn-1-yloxy)-4H-chromen-4-one

: 1467042-79-0
1-(N-β-D-galactopyranosyl)-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; sodium L-ascorbate; sodium hydrogencarbonate / dichloromethane; water / 20 °C

2: sodium methylate; methanol / 4 h / 20 °C

With methanol; copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; sodium methylate; sodium hydrogencarbonate; sodium L-ascorbate; In dichloromethane; water;
DOI:10.2174/15701786113109990039

Reference yield:

: 1098-92-6
kaempferol 5,7,4'-trimethyl ether

: 1467042-79-0
1-(N-β-D-galactopyranosyl)-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 2 h / Reflux

2: copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; sodium L-ascorbate; sodium hydrogencarbonate / dichloromethane; water / 20 °C

3: sodium methylate; methanol / 4 h / 20 °C

With methanol; copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; sodium methylate; sodium hydrogencarbonate; potassium carbonate; sodium L-ascorbate; In dichloromethane; water; acetone;
DOI:10.2174/15701786113109990039