1-[N-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)]-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

Base Information

Chemical Name:1-[N-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)]-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole
CAS No.:1467042-70-1
Molecular Formula:C₃₅H₃₇N₃O₁₅
Molecular Weight:739.69
Hs Code.:

Synonyms:1-[N-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)]-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

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Chemical Property of 1-[N-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)]-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

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Technology Process of 1-[N-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)]-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

There total 2 articles about 1-[N-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)]-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: C₁₅H₂₀N₂O₉

: 1467042-67-6
5,7-dimethoxy-2-(4-methoxyphenyl)-3-(prop-2-yn-1-yloxy)-4H-chromen-4-one

: 1467042-70-1
1-[N-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)]-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

Guidance literature:: With copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; sodium hydrogencarbonate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃; regioselective reaction;
DOI:10.2174/15701786113109990039

Reference yield:

: 1098-92-6
kaempferol 5,7,4'-trimethyl ether

: 1467042-70-1
1-[N-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)]-4-[3-O-methylene-(7,5,4’-trimethoxy flavonol)]-[1,2,3]-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 2 h / Reflux

2: copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; sodium L-ascorbate; sodium hydrogencarbonate / dichloromethane; water / 20 °C

With copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; sodium hydrogencarbonate; potassium carbonate; sodium L-ascorbate; In dichloromethane; water; acetone;
DOI:10.2174/15701786113109990039