(E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-yl benzoate

Base Information

Chemical Name:(E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-yl benzoate
CAS No.:1044846-08-3
Molecular Formula:C₃₁H₃₄O₃Si
Molecular Weight:482.695
Hs Code.:

Synonyms:(E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-yl benzoate

Suppliers and Price of (E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-yl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-yl benzoate

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Technology Process of (E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-yl benzoate

There total 1 articles about (E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1044846-00-5
(E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-ol

: 98-88-4
benzoyl chloride

: 1044846-08-3
(E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-yl benzoate

Guidance literature:: (E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-ol; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 0.583333h; Inert atmosphere;

benzoyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h;
DOI:10.1021/jo8010107

Reference yield: 73.0%

: 1044846-08-3
(E)-7-(tert-butyldiphenylsilyloxy)-3-methylhept-4-en-1-yn-3-yl benzoate

: 75-16-1
methylmagnesium bromide

: (E)-tert-butyl(5-methylocta-3,5,6-trienyloxy)diphenylsilane

Guidance literature:: With copper(l) iodide; lithium bromide; In tetrahydrofuran; at -78 - 20 ℃; for 8h; Inert atmosphere;
DOI:10.1021/jo8010107