5-chloro-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis-(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one

Base Information

• Chemical Name: 5-chloro-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis-(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one
• CAS No.: 105167-87-1
• Molecular Formula: C₃₉H₃₄ClN₃O₄
• Molecular Weight: 644.17

Synonyms:5-chloro-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis-(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one

Chemical Property of 5-chloro-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis-(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of 5-chloro-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis-(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one

There total 1 articles about 5-chloro-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis-(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

benzyl bromide (100-39-0) + 5-chloro-2-[2-[(2-hydroxyethyl)amino]ethyl]-7,10-bis(phenylmethoxy)anthra[1,9-cd]-pyrazol-6(2H)-one (91441-59-7) → 5-chloro-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis-(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one (105167-87-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 96h; Ambient temperature;

DOI:10.1002/jhet.5570260117

Reference yield: 79.0%

5-chloro-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis-(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one (105167-87-1) + Trimethylenediamine (109-76-2,54018-94-9) → 5-<(3-aminopropyl)amino>-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one (105158-35-8)

Guidance literature:

at 115 - 120 ℃; for 2.5h;

DOI:10.1002/jhet.5570260117

Reference yield: 61.0%

N-benzyl-N-methylethylenediamine (14165-18-5) + 5-chloro-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis-(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one (105167-87-1) → 2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-5-<<2-ethyl>amino>-7,10-bis(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one (105158-36-9)

Guidance literature:

at 150 ℃; for 2h;

DOI:10.1002/jhet.5570260117

upstream raw materials:

benzyl bromide

5-chloro-2-[2-[(2-hydroxyethyl)amino]ethyl]-7,10-bis(phenylmethoxy)anthra[1,9-cd]-pyrazol-6(2H)-one

Downstream raw materials:

2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-5-<<2-ethyl>amino>-7,10-bis(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one

5-<(3-aminopropyl)amino>-2-<2-<(2-hydroxyethyl)(phenylmethyl)amino>ethyl>-7,10-bis(phenylmethoxy)anthra<1,9-cd>pyrazol-6(2H)-one

7,10-dihydroxy-2-<2-<(2-hydroxyethyl)amino>ethyl>-5-<<(2-methylamino)ethyl>amino>anthra<1,9-cd>pyrazol-6(2H)-one

Piroxantrone

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