exo-5-Brom-endo-5-chlor-6-<(4-methoxyphenyl)methylen>bicyclo<2.1.1>hexan

Base Information

Chemical Name:exo-5-Brom-endo-5-chlor-6-<(4-methoxyphenyl)methylen>bicyclo<2.1.1>hexan
CAS No.:120545-94-0
Molecular Formula:C₁₄H₁₄BrClO
Molecular Weight:313.622
Hs Code.:

Synonyms:exo-5-Brom-endo-5-chlor-6-<(4-methoxyphenyl)methylen>bicyclo<2.1.1>hexan

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Chemical Property of exo-5-Brom-endo-5-chlor-6-<(4-methoxyphenyl)methylen>bicyclo<2.1.1>hexan

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Technology Process of exo-5-Brom-endo-5-chlor-6-<(4-methoxyphenyl)methylen>bicyclo<2.1.1>hexan

There total 3 articles about exo-5-Brom-endo-5-chlor-6-<(4-methoxyphenyl)methylen>bicyclo<2.1.1>hexan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 120545-75-7
(6-Bromtricyclo<3.1.0.0^2,6>hex-1-yl)(4-methoxyphenyl)methanol

: 120545-94-0
exo-5-Brom-endo-5-chlor-6-<(4-methoxyphenyl)methylen>bicyclo<2.1.1>hexan

Guidance literature:: With N-chloro-succinimide; dimethylsulfide; In dichloromethane; at 20 ℃; for 5h;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 120545-94-0
exo-5-Brom-endo-5-chlor-6-<(4-methoxyphenyl)methylen>bicyclo<2.1.1>hexan

Guidance literature:: Multi-step reaction with 3 steps

1: 1) BuLi / 1) ether, 12 h, 2) 3 h, RT

2: 1) BuLi, 2) TsBr / 1) ether, 17 h, RT, 2) 1 h, RT

3: 49 percent / N-chlorosuccinimide, Me₂S / CH₂Cl₂ / 5 h / 20 °C

With N-chloro-succinimide; n-butyllithium; dimethylsulfide; toluene-p-sulfonyl bromide; In dichloromethane;

Reference yield:

: 120545-55-3
(4-Methoxyphenyl)tricyclo<3.1.0.0^2,6>hex-1-ylmethanol

: 120545-94-0
exo-5-Brom-endo-5-chlor-6-<(4-methoxyphenyl)methylen>bicyclo<2.1.1>hexan

Guidance literature:: Multi-step reaction with 2 steps

1: 1) BuLi, 2) TsBr / 1) ether, 17 h, RT, 2) 1 h, RT

2: 49 percent / N-chlorosuccinimide, Me₂S / CH₂Cl₂ / 5 h / 20 °C

With N-chloro-succinimide; n-butyllithium; dimethylsulfide; toluene-p-sulfonyl bromide; In dichloromethane;