C₁₈H₂₂INO₆

Base Information

Chemical Name:C₁₈H₂₂INO₆
CAS No.:1450984-51-6
Molecular Formula:C₁₈H₂₂INO₆
Molecular Weight:475.28
Hs Code.:

C<sub>18</sub>H<sub>22</sub>INO<sub>6</sub>

Synonyms:C₁₈H₂₂INO₆

Suppliers and Price of C₁₈H₂₂INO₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₈H₂₂INO₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₈H₂₂INO₆

There total 10 articles about C₁₈H₂₂INO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1450984-49-2
benzyl (2R,3S,5S)-3-hydroxy-2-hydroxymethyl-5-(iodomethyl)pyrrolidine-1-carboxylate

: 75-36-5
acetyl chloride

: 1450984-51-6
C₁₈H₂₂INO₆

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c3md00033h

Reference yield:

: 6081-61-4
N-(benzyloxycarbonyl)-D-serine

: 1450984-51-6
C₁₈H₂₂INO₆

Guidance literature:: Multi-step reaction with 10 steps

1: 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1.5 h / 0 - 25 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / acetone / 15 h / 25 °C / Inert atmosphere

3: diethyl ether / 2 h / -78 °C / Inert atmosphere

4: zinc tetrahydridoborate*Et₂O; cerium(III) chloride heptahydrate / methanol / 2.5 h / 0 - 25 °C / Inert atmosphere

5: water; acetic acid / 15 h / 50 °C

6: toluene-4-sulfonic acid / acetone / 1 h / 25 °C / Inert atmosphere

7: acetonitrile / 1 h / 90 °C / Inert atmosphere

8: sodium chloride / ethyl acetate; water; acetonitrile / 1.5 h / 25 °C

9: iodine / dichloromethane / 1.5 h / 25 °C / Inert atmosphere

10: pyridine / dichloromethane / 3 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; pyridine; zinc tetrahydridoborate*Et₂O; cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; water; iodine; toluene-4-sulfonic acid; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium chloride; In methanol; diethyl ether; dichloromethane; water; ethyl acetate; acetone; acetonitrile;
DOI:10.1039/c3md00033h

Reference yield:

: 656827-13-3
(R)-benzyl-4-(methoxy(methyl)carbamoyl)-2,2-dimethyloxazolidine-3-carboxylate

: 1450984-51-6
C₁₈H₂₂INO₆

Guidance literature:: Multi-step reaction with 8 steps

1: diethyl ether / 2 h / -78 °C / Inert atmosphere

2: zinc tetrahydridoborate*Et₂O; cerium(III) chloride heptahydrate / methanol / 2.5 h / 0 - 25 °C / Inert atmosphere

3: water; acetic acid / 15 h / 50 °C

4: toluene-4-sulfonic acid / acetone / 1 h / 25 °C / Inert atmosphere

5: acetonitrile / 1 h / 90 °C / Inert atmosphere

6: sodium chloride / ethyl acetate; water; acetonitrile / 1.5 h / 25 °C

7: iodine / dichloromethane / 1.5 h / 25 °C / Inert atmosphere

8: pyridine / dichloromethane / 3 h / 0 °C / Inert atmosphere

With pyridine; zinc tetrahydridoborate*Et₂O; cerium(III) chloride heptahydrate; water; iodine; toluene-4-sulfonic acid; acetic acid; sodium chloride; In methanol; diethyl ether; dichloromethane; water; ethyl acetate; acetone; acetonitrile;
DOI:10.1039/c3md00033h