7-benzyl-4-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-7H-pyrrolo[2,3-d]pyrimidine

Base Information

Chemical Name:7-benzyl-4-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-7H-pyrrolo[2,3-d]pyrimidine
CAS No.:1143505-19-4
Molecular Formula:C₁₉H₂₁BClN₃O₂
Molecular Weight:369.659
Hs Code.:

Synonyms:7-benzyl-4-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-7H-pyrrolo[2,3-d]pyrimidine

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Chemical Property of 7-benzyl-4-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-7H-pyrrolo[2,3-d]pyrimidine

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Technology Process of 7-benzyl-4-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-7H-pyrrolo[2,3-d]pyrimidine

There total 1 articles about 7-benzyl-4-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-7H-pyrrolo[2,3-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 16019-34-4
7-benzyl-4-chloro-7H-pyrrolo[2,3-d]pyrimidine

: 73183-34-3
bis(pinacol)diborane

: 1143505-19-4
7-benzyl-4-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-7H-pyrrolo[2,3-d]pyrimidine

Guidance literature:: With [Ir(C₈H₁₂)(OCH₃)]2; (CH₃)3CC₅H₃NC₅H₃NC(CH₃)3; In tetrahydrofuran; dissolving mixt. of deazapurine deriv., boron compd., iridium compd. andbipyridine deriv. in dry THF under Ar, heating at 80°C for 20 h; evapn., chromy. (silica gel, hexane/ethyl acetate (from 5:1 to 1:1)), NMR and MS;
DOI:10.1039/b900218a

Reference yield:

: 5029-67-4
2-iodopyridine

: 1143505-19-4
7-benzyl-4-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-7H-pyrrolo[2,3-d]pyrimidine

: 1143505-36-5
7-benzyl-4-chloro-6-(pyridin-2-yl)-7H-pyrrolo[2,3-d]pyrimidine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 1h; Inert atmosphere;
DOI:10.1039/b900218a

Reference yield:

: 696-62-8
para-iodoanisole

: 1143505-19-4
7-benzyl-4-chloro-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-7H-pyrrolo[2,3-d]pyrimidine

: 1143505-35-4
7-benzyl-4-chloro-6-(4-methoxyphenyl)-7H-pyrrolo[2,3-d]pyrimidine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 1h; Inert atmosphere;
DOI:10.1039/b900218a