2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-butencarbonsaureaethylester

Base Information

Chemical Name:2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-butencarbonsaureaethylester
CAS No.:79936-88-2
Molecular Formula:C₁₆H₂₆O₂
Molecular Weight:253.357
Hs Code.:

Synonyms:2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-butencarbonsaureaethylester

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Chemical Property of 2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-butencarbonsaureaethylester

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Technology Process of 2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-butencarbonsaureaethylester

There total 7 articles about 2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-butencarbonsaureaethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 79936-85-9
2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-acetaldehyde

: 21382-82-1
(carbethoxyethylidene)triphenylphosphorane

: 79936-88-2
2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-butencarbonsaureaethylester

Guidance literature:: In benzene; for 17h; Heating;
DOI:10.1002/hlca.19810640504

Reference yield:

: 79936-76-8
C₂₀H₂₅⁽²⁾H₃O₂

: 79936-88-2
2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-butencarbonsaureaethylester

Guidance literature:: Multi-step reaction with 4 steps

1: conc. HCl / 1.17 h / Heating

2: 46 percent / MgSO₄, KMNO₄ / acetone / 2 h / Ambient temperature

4: 82 percent / benzene / 17 h / Heating

With hydrogenchloride; potassium permanganate; magnesium sulfate; In acetone; benzene;
DOI:10.1002/hlca.19810640504

Reference yield:

: 79936-77-9
2-<(1'S,2'S,6'R)-2',6'-dimethyl-2'-(2''-hydroxy-4''-isopropyl)phenyl-6'-triduteriomethyl-cyclohexyl>-essigsauremethylester

: 79936-88-2
2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-butencarbonsaureaethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / MgSO₄, KMNO₄ / acetone / 2 h / Ambient temperature

3: 82 percent / benzene / 17 h / Heating

With potassium permanganate; magnesium sulfate; In acetone; benzene;
DOI:10.1002/hlca.19810640504