2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetic acid

Base Information

Chemical Name:2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetic acid
CAS No.:1292687-92-3
Molecular Formula:C₁₈H₂₀O₄
Molecular Weight:300.354
Hs Code.:

Synonyms:2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetic acid

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Chemical Property of 2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetic acid

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Technology Process of 2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetic acid

There total 13 articles about 2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1292688-15-3
ethyl 2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate

: 1292687-92-3
2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetic acid

Guidance literature:: ethyl 2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetate; With ethanol; sodium hydroxide; at 20 ℃; for 3h;

With hydrogenchloride; In chloroform; water; pH=3.5 - 4;

Reference yield:

: 632-46-2
2,6-dimethylbenzoic acid

: 1292687-92-3
2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetic acid

Guidance literature:: Multi-step reaction with 9 steps

1.1: nitric acid; sulfuric acid / nitromethane / 21 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

3.1: tin(II) chloride dihdyrate / ethanol / 2 h / 80 °C

3.2: pH 5

4.1: water; sodium nitrite; sulfuric acid / 0 - 120 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 0 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

7.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C

9.1: sodium hydroxide; ethanol / 3 h / 20 °C

9.2: pH 3.5 - 4

With 1H-imidazole; lithium aluminium tetrahydride; tin(II) chloride dihdyrate; ethanol; di-isopropyl azodicarboxylate; sulfuric acid; tetrabutyl ammonium fluoride; water; nitric acid; potassium carbonate; triphenylphosphine; sodium hydroxide; sodium nitrite; In tetrahydrofuran; nitromethane; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 131236-69-6
methyl 2,6-dimethyl-3-hydroxybenzene-1-carboxylate

: 1292687-92-3
2-(3-(3-hydroxy-2,6-dimethylbenzyloxy)-4-methylphenyl)acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 0 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C

5.1: sodium hydroxide; ethanol / 3 h / 20 °C

5.2: pH 3.5 - 4

With 1H-imidazole; lithium aluminium tetrahydride; ethanol; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;