Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4-(4-methoxy-phenyl)-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

Base Information

Chemical Name:Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4-(4-methoxy-phenyl)-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate
CAS No.:105199-42-6
Molecular Formula:C₂₂H₂₁N₂O₄S*Na
Molecular Weight:432.476
Hs Code.:

Synonyms:Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4-(4-methoxy-phenyl)-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

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Chemical Property of Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4-(4-methoxy-phenyl)-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

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Technology Process of Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4-(4-methoxy-phenyl)-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

There total 1 articles about Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4-(4-methoxy-phenyl)-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 7357-70-2
Cyanothioacetamide

: 148345-21-5
(Z)-ethyl 2-benzoyl-3-(4'-methoxyphenyl)-2-propenoate

: 105199-42-6
Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4-(4-methoxy-phenyl)-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

Guidance literature:: With sodium methylate; In methanol; for 24h; Ambient temperature;

Reference yield: 50.0%

: 105199-42-6
Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4-(4-methoxy-phenyl)-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

: 105199-52-8
5-Cyano-4-(4-methoxy-phenyl)-2-phenyl-6-thioxo-1,4,5,6-tetrahydro-pyridine-3-carboxylic acid ethyl ester

Guidance literature:: With acetic acid; In water;

Reference yield:

: 105199-42-6
Sodium; (4R,5S,6R)-3-cyano-5-ethoxycarbonyl-6-hydroxy-4-(4-methoxy-phenyl)-6-phenyl-1,4,5,6-tetrahydro-pyridine-2-thiolate

: 105199-57-3
C₄₄H₃₄N₄O₆S₂

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / acetic acid / H₂O

2: 81 percent / nitrosylsulfuric acid / acetic acid / 1 h / 0 °C

With nitrosylsulfuric acid; acetic acid; In water; acetic acid;