C₁₅H₂₀O₃

Base Information

• Chemical Name: C₁₅H₂₀O₃
• CAS No.: 1330640-57-7
• Molecular Formula: C₁₅H₂₀O₃
• Molecular Weight: 248.322
• Mol file: 1330640-57-7.mol

Synonyms:C₁₅H₂₀O₃

Chemical Property of C₁₅H₂₀O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₅H₂₀O₃

There total 1 articles about C₁₅H₂₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2,3-dihydro-2H-furan (1191-99-7,75454-45-4) + (2R)-1-(benzyloxy)but-3-en-2-ol (93553-66-3,109613-59-4,114819-44-2,113426-94-1) → C15H20O3 (1330640-57-7)

Guidance literature:

With pyridinium p-toluenesulfonate; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1039/c1cc12934a

Reference yield:

C15H20O3 (1330640-57-7) + triethylsilyl trifluoromethyl sulfonate (79271-56-0) + allyl alcohol (107-18-6) → C25H42O4Si

Guidance literature:

C₁₅H₂₀O₃; triethylsilyl trifluoromethyl sulfonate; With 2,4,6-trimethyl-pyridine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

allyl alcohol; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c1cc12934a

Reference yield:

C15H20O3 (1330640-57-7) → C18H26O4 (1330640-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 2,4,6-trimethyl-pyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 2 h / 0 °C

With 2,4,6-trimethyl-pyridine; potassium carbonate; In methanol; dichloromethane;

DOI:10.1039/c1cc12934a

upstream raw materials:

2,3-dihydro-2H-furan

(2R)-1-(benzyloxy)but-3-en-2-ol

Downstream raw materials:

C₁₈H₂₆O₄

C₂₅H₃₀O₅

C₂₃H₂₆O₅

C₂₃H₂₆O₅