N-[(2,6-difluoro-4-methoxyphenyl)methylene]-6-(trifluoromethyl)-3-pyridinamine

Base Information

• Chemical Name: N-[(2,6-difluoro-4-methoxyphenyl)methylene]-6-(trifluoromethyl)-3-pyridinamine
• CAS No.: 1193511-88-4
• Molecular Formula: C₁₄H₉F₅N₂O
• Molecular Weight: 316.23

Synonyms:N-[(2,6-difluoro-4-methoxyphenyl)methylene]-6-(trifluoromethyl)-3-pyridinamine

Chemical Property of N-[(2,6-difluoro-4-methoxyphenyl)methylene]-6-(trifluoromethyl)-3-pyridinamine

Chemical Property:

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Technology Process of N-[(2,6-difluoro-4-methoxyphenyl)methylene]-6-(trifluoromethyl)-3-pyridinamine

There total 1 articles about N-[(2,6-difluoro-4-methoxyphenyl)methylene]-6-(trifluoromethyl)-3-pyridinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-difluoro-4-methoxybenzaldehyde (256417-10-4) + 6-(trifluoromethyl)pyridin-3-amine (106877-33-2) → N-[(2,6-difluoro-4-methoxyphenyl)methylene]-6-(trifluoromethyl)-3-pyridinamine (1193511-88-4)

Guidance literature:

In toluene; for 60h; Reflux;

Reference yield:

N-[(2,6-difluoro-4-methoxyphenyl)methylene]-6-(trifluoromethyl)-3-pyridinamine (1193511-88-4) + [(p-methylphenyl)sulfonylmethyl]isonitrile (38622-91-2,36635-61-7) → 5-[5-(2,6-difluoro-4-methoxyphenyl)-1H-imidazol-1-yl]-2-(trifluoromethyl)pyridine (1193512-02-5)

Guidance literature:

With potassium carbonate; In methanol; 1,2-dimethoxyethane; at 75 ℃;

Reference yield:

N-[(2,6-difluoro-4-methoxyphenyl)methylene]-6-(trifluoromethyl)-3-pyridinamine (1193511-88-4) + 1-(toluene-4-sulfonyl)-ethyl isocyanide (58379-80-9) → 5-[5-(2,6-difluoro-4-methoxyphenyl)-1H-imidazol-1-yl]-2-(trifluoromethyl)pyridine (1193512-02-5)

Guidance literature:

With potassium carbonate; In methanol; 1,2-dimethoxyethane; at 75 ℃;

upstream raw materials:

2,6-difluoro-4-methoxybenzaldehyde

6-(trifluoromethyl)pyridin-3-amine

Downstream raw materials:

5-[5-(2,6-difluoro-4-methoxyphenyl)-1H-imidazol-1-yl]-2-(trifluoromethyl)pyridine

5-[4-chloro-5-(2,6-difluoro-4-methoxyphenyl)-1H-imidazol-1-yl]-2-(trifluoromethyl)pyridine

5-[2-bromo-4-chloro-5-(2,6-difluoro-4-methoxyphenyl)-1H-imidazol-1-yl]-2-(trifluoromethyl)pyridine

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