5-(methoxycarbonyl)pentyl 2-trichloroacetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:5-(methoxycarbonyl)pentyl 2-trichloroacetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside
CAS No.:1446762-32-8
Molecular Formula:C₂₂H₂₈Cl₃NO₈
Molecular Weight:540.825
Hs Code.:

Synonyms:5-(methoxycarbonyl)pentyl 2-trichloroacetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

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Chemical Property of 5-(methoxycarbonyl)pentyl 2-trichloroacetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Chemical Property:

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Technology Process of 5-(methoxycarbonyl)pentyl 2-trichloroacetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

There total 4 articles about 5-(methoxycarbonyl)pentyl 2-trichloroacetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: C₁₅H₂₄Cl₃NO₈

: 1446762-32-8
5-(methoxycarbonyl)pentyl 2-trichloroacetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In acetonitrile; at 0 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/asia.201201204

Reference yield:

: 1446762-39-5
C₂₁H₃₀Cl₃NO₁₁

: 1446762-32-8
5-(methoxycarbonyl)pentyl 2-trichloroacetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 1 h / 20 °C / Inert atmosphere

2: camphor-10-sulfonic acid / acetonitrile / 5 h / 0 - 20 °C / Inert atmosphere

With camphor-10-sulfonic acid; sodium methylate; In methanol; acetonitrile;
DOI:10.1002/asia.201201204

Reference yield:

: 219693-02-4
1,3,4,6-tetra-O-acetyl-2-deoxy-2-trichloroacetamido-α/β-D-glucopyranose

: 1446762-32-8
5-(methoxycarbonyl)pentyl 2-trichloroacetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere

2.1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 0.5 h / 0 °C / Inert atmosphere

3.1: sodium methylate / methanol / 1 h / 20 °C / Inert atmosphere

4.1: camphor-10-sulfonic acid / acetonitrile / 5 h / 0 - 20 °C / Inert atmosphere

With camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium methylate; In methanol; dichloromethane; acetonitrile;
DOI:10.1002/asia.201201204