3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoic acid 2-acetylhydrazide

Base Information

Chemical Name:3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoic acid 2-acetylhydrazide
CAS No.:134472-33-6
Molecular Formula:C₁₈H₂₃N₃O₄
Molecular Weight:345.398
Hs Code.:

Synonyms:3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoic acid 2-acetylhydrazide

Suppliers and Price of 3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoic acid 2-acetylhydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoic acid 2-acetylhydrazide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoic acid 2-acetylhydrazide

There total 5 articles about 3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoic acid 2-acetylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34137-14-9
methyl 4-hydroxy-3,5-dimethylbenzoate

: 134472-33-6
3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoic acid 2-acetylhydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 98.2 percent / K₂CO₃, KI / various solvent(s) / 24 h / 65 °C

2: 95.4 percent / H₂O, NaOH / ethanol / 1 h / Heating

3: 1.) CDI / 1.) THF, reflux, 2 h, 2.) THF, reflux, 22 h

With sodium hydroxide; water; potassium carbonate; 1,1'-carbonyldiimidazole; potassium iodide; In ethanol;
DOI:10.1021/jm00041a022

Reference yield:

: 130800-76-9
3-(3-methylisoxazol-5-yl)propyl chloride

: 134472-33-6
3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoic acid 2-acetylhydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 98.2 percent / K₂CO₃, KI / various solvent(s) / 24 h / 65 °C

2: 95.4 percent / H₂O, NaOH / ethanol / 1 h / Heating

3: 1.) CDI / 1.) THF, reflux, 2 h, 2.) THF, reflux, 22 h

With sodium hydroxide; water; potassium carbonate; 1,1'-carbonyldiimidazole; potassium iodide; In ethanol;
DOI:10.1021/jm00041a022

Reference yield:

: 156787-33-6
methyl 3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoate

: 134472-33-6
3,5-dimethyl-4-<<3-(3-methyl-5-isoxazolyl)propyl>oxy>benzoic acid 2-acetylhydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 95.4 percent / H₂O, NaOH / ethanol / 1 h / Heating

2: 1.) CDI / 1.) THF, reflux, 2 h, 2.) THF, reflux, 22 h

With sodium hydroxide; water; 1,1'-carbonyldiimidazole; In ethanol;
DOI:10.1021/jm00041a022