1-(3,4-dimethoxybenzyl)-3,4,5,6,7,8-hexahydroisoquinoline hydrochloride

Base Information

Chemical Name:1-(3,4-dimethoxybenzyl)-3,4,5,6,7,8-hexahydroisoquinoline hydrochloride
CAS No.:101781-78-6
Molecular Formula:C₁₈H₂₃NO₂*ClH
Molecular Weight:321.847
Hs Code.:

Synonyms:1-(3,4-dimethoxybenzyl)-3,4,5,6,7,8-hexahydroisoquinoline hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3,4-dimethoxybenzyl)-3,4,5,6,7,8-hexahydroisoquinoline hydrochloride

Chemical Property:

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Technology Process of 1-(3,4-dimethoxybenzyl)-3,4,5,6,7,8-hexahydroisoquinoline hydrochloride

There total 3 articles about 1-(3,4-dimethoxybenzyl)-3,4,5,6,7,8-hexahydroisoquinoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 101864-71-5
N-<2-(1-cyclohexenyl)ethyl>-3,4-dimethoxyphenylacetamide

: 101781-78-6
1-(3,4-dimethoxybenzyl)-3,4,5,6,7,8-hexahydroisoquinoline hydrochloride

Guidance literature:: With phosphorus pentachloride; In chloroform; for 6h; Ambient temperature;
DOI:10.1016/0223-5234(91)90195-S

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 101781-78-6
1-(3,4-dimethoxybenzyl)-3,4,5,6,7,8-hexahydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 3 h / 180 - 200 °C

2: 72 percent / PCl₅ / CHCl₃ / 6 h / Ambient temperature

With phosphorus pentachloride; In chloroform;
DOI:10.1016/0223-5234(91)90195-S

Reference yield:

: 3399-73-3
2-(1-cyclohexenyl)ethylamine

: 101781-78-6
1-(3,4-dimethoxybenzyl)-3,4,5,6,7,8-hexahydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 3 h / 180 - 200 °C

2: 72 percent / PCl₅ / CHCl₃ / 6 h / Ambient temperature

With phosphorus pentachloride; In chloroform;
DOI:10.1016/0223-5234(91)90195-S