C₂₁H₂₂N₆O₄

Base Information

Chemical Name:C₂₁H₂₂N₆O₄
CAS No.:1325711-77-0
Molecular Formula:C₂₁H₂₂N₆O₄
Molecular Weight:422.443
Hs Code.:

C<sub>21</sub>H<sub>22</sub>N<sub>6</sub>O<sub>4</sub>

Synonyms:C₂₁H₂₂N₆O₄

Suppliers and Price of C₂₁H₂₂N₆O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₁H₂₂N₆O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₁H₂₂N₆O₄

There total 5 articles about C₂₁H₂₂N₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1325711-76-9
C₁₃H₁₂ClN₅O₃

: 2393-23-9
4-methoxy-benzylamine

: 1325711-77-0
C₂₁H₂₂N₆O₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In propan-1-ol; at 70 ℃; for 4h;
DOI:10.1002/cmdc.201100126

Reference yield:

: 2004-06-0
6-Chloropurine riboside

: 1325711-77-0
C₂₁H₂₂N₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / acetone / 2 h / 20 °C

2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / water; acetonitrile / 4 h / 40 °C / Inert atmosphere

3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium chloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 50 °C

4: oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / -78 °C

5: N-ethyl-N,N-diisopropylamine / propan-1-ol / 4 h / 70 °C

With oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium chloride; benzotriazol-1-ol; toluene-4-sulfonic acid; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In propan-1-ol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1002/cmdc.201100126

Reference yield:

: 39824-26-5
6-chloro-9-(2,3-O-isopropylidene-β-D-ribofuranosyl)-9H-purine

: 1325711-77-0
C₂₁H₂₂N₆O₄

Guidance literature:: Multi-step reaction with 4 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / water; acetonitrile / 4 h / 40 °C / Inert atmosphere

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium chloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 50 °C

3: oxalyl dichloride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / -78 °C

4: N-ethyl-N,N-diisopropylamine / propan-1-ol / 4 h / 70 °C

With oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium chloride; benzotriazol-1-ol; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In propan-1-ol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201100126