(R)-1-acetoxy-2-<3-(allyloxy)phenyl>-3-<(tetrahydropyran-2-yl)oxy>propane

Base Information

Chemical Name:(R)-1-acetoxy-2-<3-(allyloxy)phenyl>-3-<(tetrahydropyran-2-yl)oxy>propane
CAS No.:183800-17-1
Molecular Formula:C₁₉H₂₆O₅
Molecular Weight:334.412
Hs Code.:

Synonyms:(R)-1-acetoxy-2-<3-(allyloxy)phenyl>-3-<(tetrahydropyran-2-yl)oxy>propane

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Chemical Property of (R)-1-acetoxy-2-<3-(allyloxy)phenyl>-3-<(tetrahydropyran-2-yl)oxy>propane

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Technology Process of (R)-1-acetoxy-2-<3-(allyloxy)phenyl>-3-<(tetrahydropyran-2-yl)oxy>propane

There total 5 articles about (R)-1-acetoxy-2-<3-(allyloxy)phenyl>-3-<(tetrahydropyran-2-yl)oxy>propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-37-4
m-hydroxyphenylacetic acid

: 183800-17-1
(R)-1-acetoxy-2-<3-(allyloxy)phenyl>-3-<(tetrahydropyran-2-yl)oxy>propane

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / H₂SO₄ / Heating

2: 96 percent / K₂CO₃ / 4 h / 55 °C

3: 90 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

4: 63 percent / DIBALH / CH₂Cl₂ / 0 °C / to room temperature

5: 3A molecular sieves / PPL / 24 h / 0 °C

6: p-TSA / CH₂Cl₂ / Ambient temperature

With 3 A molecular sieve; sulfuric acid; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; lithium diisopropyl amide; PPL; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)61382-5

Reference yield:

: 22446-38-4
ethyl 3-hydroxyphenylacetate

: 183800-17-1
(R)-1-acetoxy-2-<3-(allyloxy)phenyl>-3-<(tetrahydropyran-2-yl)oxy>propane

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / K₂CO₃ / 4 h / 55 °C

2: 90 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

3: 63 percent / DIBALH / CH₂Cl₂ / 0 °C / to room temperature

4: 3A molecular sieves / PPL / 24 h / 0 °C

5: p-TSA / CH₂Cl₂ / Ambient temperature

With 3 A molecular sieve; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; lithium diisopropyl amide; PPL; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)61382-5

Reference yield:

: 169888-83-9
3-allyloxyphenyl acetic acid ethyl ester

: 183800-17-1
(R)-1-acetoxy-2-<3-(allyloxy)phenyl>-3-<(tetrahydropyran-2-yl)oxy>propane

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

2: 63 percent / DIBALH / CH₂Cl₂ / 0 °C / to room temperature

3: 3A molecular sieves / PPL / 24 h / 0 °C

4: p-TSA / CH₂Cl₂ / Ambient temperature

With 3 A molecular sieve; diisobutylaluminium hydride; toluene-4-sulfonic acid; lithium diisopropyl amide; PPL; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)61382-5