(E)-methyl 3-(1-phenylbut-3-enyloxy)acrylate

Base Information

Chemical Name:(E)-methyl 3-(1-phenylbut-3-enyloxy)acrylate
CAS No.:1283728-10-8
Molecular Formula:C₁₄H₁₆O₃
Molecular Weight:232.279
Hs Code.:

Synonyms:(E)-methyl 3-(1-phenylbut-3-enyloxy)acrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-methyl 3-(1-phenylbut-3-enyloxy)acrylate

Chemical Property:

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Technology Process of (E)-methyl 3-(1-phenylbut-3-enyloxy)acrylate

There total 7 articles about (E)-methyl 3-(1-phenylbut-3-enyloxy)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: C₁₄H₁₅IO₃

: 1283728-10-8
(E)-methyl 3-(1-phenylbut-3-enyloxy)acrylate

Guidance literature:: With (1,2-dimethoxyethane)dichloronickel(II); zinc; 2,6-bis(4,5-dihydrooxazol-2-yl)pyridine; In methanol; at 40 ℃; for 2h;
DOI:10.1021/ol200455n

Reference yield:

: (E)-methyl 3-(4-iodo-1-phenylbutoxy)acrylate

: 1283728-08-4
(E)-methyl 3-(1-phenylbutoxy)acrylate

: 1283728-10-8
(E)-methyl 3-(1-phenylbut-3-enyloxy)acrylate

: 1283728-09-5
(E)-methyl 7-hydroxy-7-phenylhept-2-enoate

: methyl 2-((2RS,6SR)-6-phenyltetrahydro-2H-pyran-2-yl)acetate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; zinc; In 2,4-dichlorophenoxyacetic acid dimethylamine; at 40 ℃; for 4h; diastereoselective reaction;
DOI:10.1021/ol200455n

Reference yield:

: 25333-24-8
3-benzoylpropionic acid methyl ester

: 1283728-08-4
(E)-methyl 3-(1-phenylbutoxy)acrylate

: 1283728-10-8
(E)-methyl 3-(1-phenylbut-3-enyloxy)acrylate

: methyl 2-((2RS,6SR)-6-phenyltetrahydro-2H-pyran-2-yl)acetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / methanol; water / 0 - 25 °C

1.2: 25 °C

2.1: 1H-imidazole / dichloromethane / 1 h / 25 °C

3.1: 4-methyl-morpholine / dichloromethane / 2 h / 25 °C

4.1: hydrogenchloride / methanol; water / 0.33 h / 25 °C

5.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 2 h / 0 °C

6.1: pyridine; nickel dichloride; zinc / tetrahydrofuran / 24 h / 60 °C

With 4-methyl-morpholine; pyridine; 1H-imidazole; hydrogenchloride; sodium tetrahydroborate; iodine; triphenylphosphine; nickel dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ol200455n