(4R,6S)-8-(benzyloxy)-4,6-dihydroxy-4-methyl-2-methylene-1-octyl acetate

Base Information

Chemical Name:(4R,6S)-8-(benzyloxy)-4,6-dihydroxy-4-methyl-2-methylene-1-octyl acetate
CAS No.:1263293-05-5
Molecular Formula:C₁₉H₂₈O₅
Molecular Weight:336.428
Hs Code.:

Synonyms:(4R,6S)-8-(benzyloxy)-4,6-dihydroxy-4-methyl-2-methylene-1-octyl acetate

Suppliers and Price of (4R,6S)-8-(benzyloxy)-4,6-dihydroxy-4-methyl-2-methylene-1-octyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,6S)-8-(benzyloxy)-4,6-dihydroxy-4-methyl-2-methylene-1-octyl acetate

Chemical Property:

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Technology Process of (4R,6S)-8-(benzyloxy)-4,6-dihydroxy-4-methyl-2-methylene-1-octyl acetate

There total 1 articles about (4R,6S)-8-(benzyloxy)-4,6-dihydroxy-4-methyl-2-methylene-1-octyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 910488-36-7
(4S)-6-(benzyloxy)-4-hydroxyhexan-2-one

: 72047-94-0
[2-(acetoxymethyl)prop-2-enyl]trimethylsilane

: 1263293-05-5
(4R,6S)-8-(benzyloxy)-4,6-dihydroxy-4-methyl-2-methylene-1-octyl acetate

Guidance literature:: [2-(acetoxymethyl)prop-2-enyl]trimethylsilane; With tin(IV) chloride; In dichloromethane; at 25 ℃;

(4S)-6-(benzyloxy)-4-hydroxyhexan-2-one; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1002/chem.201002204

Reference yield:

: 1263293-05-5
(4R,6S)-8-(benzyloxy)-4,6-dihydroxy-4-methyl-2-methylene-1-octyl acetate

: 325172-30-3
(S)-3-((tert-butyldimethylsilyl)oxy)-5-((4-methoxybenzyl)oxy)pentanal

: (3S,5R,9R,11S)-1-(benzyloxy)-11-(tert-butyldimethylsilyloxy)-13-(4-methoxybenzyloxy)-5-methyl-7-methylenetridecane-3,5,9-triol

: (3S,5R,9S,11S)-1-(benzyloxy)-11-(tert-butyldimethylsilyloxy)-13-(4-methoxybenzyloxy)-5-methyl-7-methylenetridecane-3,5,9-triol

Guidance literature:: (4R,6S)-8-(benzyloxy)-4,6-dihydroxy-4-methyl-2-methylene-1-octyl acetate; (S)-3-((tert-butyl)dimethylsilyloxy)-5-(4-methoxybenzyloxy)pentanal; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In dimethyl sulfoxide; at 25 ℃; for 0.166667h;

With bis(pinacol)diborane; In dimethyl sulfoxide; at 25 ℃; optical yield given as %de;
DOI:10.1002/chem.201002204