N-allyl-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-iodobenzyl)prop-2-en-1-amine

Base Information

Chemical Name:N-allyl-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-iodobenzyl)prop-2-en-1-amine
CAS No.:1321992-81-7
Molecular Formula:C₁₈H₂₀F₆INO₂
Molecular Weight:523.257
Hs Code.:

Synonyms:N-allyl-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-iodobenzyl)prop-2-en-1-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-allyl-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-iodobenzyl)prop-2-en-1-amine

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Technology Process of N-allyl-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-iodobenzyl)prop-2-en-1-amine

There total 5 articles about N-allyl-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-iodobenzyl)prop-2-en-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1321992-80-6
4-(bromomethyl)-2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodobenzene

: 124-02-7
diallylamine

: 1321992-81-7
N-allyl-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-iodobenzyl)prop-2-en-1-amine

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; at 80 ℃; Inert atmosphere;

Reference yield:

: 1992-07-0
4-methyl-2-<1-hydroxy-1-(trifluoromethyl)-2,2,2-trifluoroethyl>aniline

: 1321992-81-7
N-allyl-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-iodobenzyl)prop-2-en-1-amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium nitrite; sulfuric acid / water / 0 °C

1.2: 80 °C / Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / 20 °C / Cooling with ice

3.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 15 h / 78 °C / Inert atmosphere

4.1: potassium carbonate; potassium iodide / acetonitrile / 80 °C / Inert atmosphere

With N-Bromosuccinimide; sulfuric acid; potassium carbonate; N-ethyl-N,N-diisopropylamine; potassium iodide; sodium nitrite; dibenzoyl peroxide; In tetrachloromethane; water; acetonitrile;

Reference yield:

: 1321992-74-8
2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene

: 1321992-81-7
N-allyl-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-iodobenzyl)prop-2-en-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 15 h / 78 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / acetonitrile / 80 °C / Inert atmosphere

With N-Bromosuccinimide; potassium carbonate; potassium iodide; dibenzoyl peroxide; In tetrachloromethane; acetonitrile;