(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)phenyl)methanamine

Base Information

Chemical Name:(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)phenyl)methanamine
CAS No.:1321992-83-9
Molecular Formula:C₂₄H₃₉F₆NO₂Sn
Molecular Weight:606.28
Hs Code.:

Synonyms:(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)phenyl)methanamine

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Chemical Property of (3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)phenyl)methanamine

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Technology Process of (3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)phenyl)methanamine

There total 7 articles about (3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)phenyl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1321992-82-8
N-allyl-N-(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)benzyl)prop-2-en-1-amine

: 1321992-83-9
(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)phenyl)methanamine

Guidance literature:: With 1,3-dimethylbarbituric acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; at 35 ℃; for 4h; Inert atmosphere;

Reference yield:

: 1321992-80-6
4-(bromomethyl)-2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodobenzene

: 1321992-83-9
(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)phenyl)methanamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; potassium iodide / acetonitrile / 80 °C / Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 4 h / 35 °C / Inert atmosphere

With n-butyllithium; 1,3-dimethylbarbituric acid; potassium carbonate; potassium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; dichloromethane; acetonitrile;

Reference yield:

: 1321992-74-8
2-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-1-iodo-4-methylbenzene

: 1321992-83-9
(3-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-4-(tributylstannyl)phenyl)methanamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 15 h / 78 °C / Inert atmosphere

2.1: potassium carbonate; potassium iodide / acetonitrile / 80 °C / Inert atmosphere

3.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 4 h / 35 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; 1,3-dimethylbarbituric acid; potassium carbonate; potassium iodide; dibenzoyl peroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; tetrachloromethane; hexane; dichloromethane; acetonitrile;