tert-butyl 2-((1-(tert-butoxycarbonyl)-1H-indol-5-yl)amino)-4-phenethylbenzoate

Base Information

Chemical Name:tert-butyl 2-((1-(tert-butoxycarbonyl)-1H-indol-5-yl)amino)-4-phenethylbenzoate
CAS No.:910242-48-7
Molecular Formula:C₃₂H₃₆N₂O₄
Molecular Weight:512.649
Hs Code.:

Synonyms:tert-butyl 2-((1-(tert-butoxycarbonyl)-1H-indol-5-yl)amino)-4-phenethylbenzoate

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Chemical Property of tert-butyl 2-((1-(tert-butoxycarbonyl)-1H-indol-5-yl)amino)-4-phenethylbenzoate

Chemical Property:

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Technology Process of tert-butyl 2-((1-(tert-butoxycarbonyl)-1H-indol-5-yl)amino)-4-phenethylbenzoate

There total 5 articles about tert-butyl 2-((1-(tert-butoxycarbonyl)-1H-indol-5-yl)amino)-4-phenethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 890315-80-7
tert-butyl 2-amino-4-phenethylbenzoate

: 182344-70-3
5-bromo-indole-1-carboxylic acid tert-butyl ester

: 910242-48-7
tert-butyl 2-((1-(tert-butoxycarbonyl)-1H-indol-5-yl)amino)-4-phenethylbenzoate

Guidance literature:: With caesium carbonate; XPhos; palladium diacetate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In toluene; at 20 ℃; for 18h; Heating / reflux;

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 910242-48-7
tert-butyl 2-((1-(tert-butoxycarbonyl)-1H-indol-5-yl)amino)-4-phenethylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate / palladium diacetate; tetrabutylammomium bromide / ISOPROPYLAMIDE / 6 h / 20 - 110 °C

2: hydrogen / 5%-palladium/activated carbon / methanol; ethyl acetate / 2 h / 20 °C

3: caesium carbonate; XPhos / palladium diacetate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 18 h / 20 °C / Heating / reflux

With hydrogen; sodium acetate; caesium carbonate; XPhos; palladium diacetate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 5%-palladium/activated carbon; tetrabutylammomium bromide; In methanol; ISOPROPYLAMIDE; ethyl acetate; toluene;

Reference yield:

: 890315-79-4
tert-butyl 2-nitro-4-((E)-2-phenylvinyl)benzoate

: 910242-48-7
tert-butyl 2-((1-(tert-butoxycarbonyl)-1H-indol-5-yl)amino)-4-phenethylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / 5%-palladium/activated carbon / methanol; ethyl acetate / 2 h / 20 °C

2: caesium carbonate; XPhos / palladium diacetate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 18 h / 20 °C / Heating / reflux

With hydrogen; caesium carbonate; XPhos; palladium diacetate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 5%-palladium/activated carbon; In methanol; ethyl acetate; toluene;