2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetramethanethiol, 1,21,23,25-tetrakis(2-phenylethyl)-

Base Information

• Chemical Name: 2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetramethanethiol, 1,21,23,25-tetrakis(2-phenylethyl)-
• CAS No.: 132352-03-5
• Molecular Formula: C₆₈H₆₄O₈S₄
• Molecular Weight: 1137.52

Synonyms:2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetramethanethiol, 1,21,23,25-tetrakis(2-phenylethyl)-

Chemical Property of 2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetramethanethiol, 1,21,23,25-tetrakis(2-phenylethyl)-

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Technology Process of 2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetramethanethiol, 1,21,23,25-tetrakis(2-phenylethyl)-

There total 1 articles about 2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetramethanethiol, 1,21,23,25-tetrakis(2-phenylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetrakis(chloromethyl)-1,21,23,25-tetrakis(2-phenylethyl)- (132352-02-4) → 2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetramethanethiol, 1,21,23,25-tetrakis(2-phenylethyl)- (132352-03-5)

Guidance literature:

With thiourea; In N,N-dimethyl-formamide; at 80 ℃; for 12h;

Reference yield: 22.0%

methanol (67-56-1) + 2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetrakis(chloromethyl)-1,21,23,25-tetrakis(2-phenylethyl)- (132352-02-4) + 2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetramethanethiol, 1,21,23,25-tetrakis(2-phenylethyl)- (132352-03-5) → C136H120O16S4*2CH4O (132881-63-1)

Guidance literature:

With rubidium carbonate; In benzene; for 24h; Heating;

Reference yield:

2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetrakis(chloromethyl)-1,21,23,25-tetrakis(2-phenylethyl)- (132352-02-4) + 2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetramethanethiol, 1,21,23,25-tetrakis(2-phenylethyl)- (132352-03-5) + acetonitrile (75-05-8,26809-02-9) → C136H120O16S4*2C2H3N (132774-92-6,132880-43-4) + C136H120O16S4*C2H3N (132774-92-6)

Guidance literature:

With rubidium carbonate; In benzene; for 24h; Heating;

upstream raw materials:

2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>bis<1,3>benzodioxocin, 7,11,15,28-tetrakis(chloromethyl)-1,21,23,25-tetrakis(2-phenylethyl)-

Downstream raw materials:

C₁₃₆H₁₂₀O₁₆S₄*2CH₄O

C₁₃₆H₁₂₀O₁₆S₄*2C₂H₃N

C₁₃₆H₁₂₀O₁₆S₄*C₂H₃N

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