4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-isophthaloyl dichloride

Base Information

Chemical Name:4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-isophthaloyl dichloride
CAS No.:773866-29-8
Molecular Formula:C₂₂H₃₂Cl₂O₁₀
Molecular Weight:527.396
Hs Code.:

Synonyms:4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-isophthaloyl dichloride

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Chemical Property of 4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-isophthaloyl dichloride

Chemical Property:

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Technology Process of 4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-isophthaloyl dichloride

There total 4 articles about 4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-isophthaloyl dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 492465-50-6
4,6-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}isophthalic acid

: 773866-29-8
4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-isophthaloyl dichloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; for 1h;
DOI:10.1021/ja0474547

Reference yield:

: 874210-29-4
4,6-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}isophthalic acid dimethyl ester

: 773866-29-8
4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-isophthaloyl dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / KOH / H₂O / 3 h / 80 °C

2: oxalyl chloride; DMF / CH₂Cl₂

With potassium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; water;
DOI:10.1021/jo050798a

Reference yield:

: 19829-74-4
4,6-dihydroxyisophthalic acid

: 773866-29-8
4,6-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-isophthaloyl dichloride

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / Heating

2: 85.4 percent / K₂CO₃ / dimethylformamide / 48 h / 100 °C

3: 91 percent / KOH / H₂O / 3 h / 80 °C

4: oxalyl chloride; DMF / CH₂Cl₂

With potassium hydroxide; oxalyl dichloride; sulfuric acid; potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo050798a