N-methoxy-N-methyl-3-(2-methyl-propane-2-sulfinylamino)-3-phenyl-propionamide

Base Information

• Chemical Name: N-methoxy-N-methyl-3-(2-methyl-propane-2-sulfinylamino)-3-phenyl-propionamide
• CAS No.: 849404-72-4
• Molecular Formula: C₁₅H₂₄N₂O₃S
• Molecular Weight: 312.433

Synonyms:N-methoxy-N-methyl-3-(2-methyl-propane-2-sulfinylamino)-3-phenyl-propionamide

Chemical Property of N-methoxy-N-methyl-3-(2-methyl-propane-2-sulfinylamino)-3-phenyl-propionamide

Chemical Property:

Purity/Quality:

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Technology Process of N-methoxy-N-methyl-3-(2-methyl-propane-2-sulfinylamino)-3-phenyl-propionamide

There total 1 articles about N-methoxy-N-methyl-3-(2-methyl-propane-2-sulfinylamino)-3-phenyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-Methoxy-N-methylacetamide (78191-00-1) + (S,E)-N-benzylidene-tert-butylsulfinamide (186249-74-1) → N-methoxy-N-methyl-3-(2-methyl-propane-2-sulfinylamino)-3-phenyl-propionamide + N-methoxy-N-methyl-3-(2-methyl-propane-2-sulfinylamino)-3-phenyl-propionamide (849404-72-4)

Guidance literature:

With potassium hexamethylsilazane; In diethyl ether; toluene; at -78 ℃; for 2h; Title compound not separated from byproducts;

DOI:10.1021/jo0402780

Reference yield: 81.0%

methylmagnesium chloride (676-58-4) + N-methoxy-N-methyl-3-(2-methyl-propane-2-sulfinylamino)-3-phenyl-propionamide (849404-72-4) → 2-Methyl-propane-2-sulfinic acid ((R)-3-oxo-1-phenyl-butyl)-amide (849404-83-7)

Guidance literature:

In tetrahydrofuran; at -78 - 20 ℃; for 3h;

DOI:10.1021/jo0402780

upstream raw materials:

N-Methoxy-N-methylacetamide

(S,E)-N-benzylidene-tert-butylsulfinamide

Downstream raw materials:

2-Methyl-propane-2-sulfinic acid ((R)-3-oxo-1-phenyl-butyl)-amide

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