(23S,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

Base Information

Chemical Name:(23S,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)
CAS No.:1226764-20-0
Molecular Formula:C₃₆H₅₁NO₄
Molecular Weight:561.805
Hs Code.:

Synonyms:(23S,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

Suppliers and Price of (23S,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (23S,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (23S,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

There total 7 articles about (23S,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1226764-22-2
C₅₁H₈₇NO₄Si₃

: 1226764-21-1
(23R,25S)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

: 1226764-19-7
(23R,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

: 1226764-18-6
(23S,25S)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

: 1226764-20-0
(23S,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

Guidance literature:: C₅₁H₈₇NO₄Si₃; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 50 ℃; for 3h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water;

Reference yield:

: 3217-93-4
N-phenylethylhydroxylamine

: 1226764-21-1
(23R,25S)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

: 1226764-19-7
(23R,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

: 1226764-18-6
(23S,25S)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

: 1226764-20-0
(23S,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: toluene / 4 h / 90 °C / Inert atmosphere

3: water; molybdenum hexacarbonyl / acetonitrile / 19 h / 80 °C

4: dichloromethane / 18 h / 20 °C / Inert atmosphere

5: triethylamine / triphenylphosphine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex / toluene / 2 h / 120 °C / Inert atmosphere

6: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 50 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; water; triethylamine; molybdenum hexacarbonyl; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;

Reference yield:

: C₂₇H₃₈BrNO₂

: 1226764-21-1
(23R,25S)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

: 1226764-19-7
(23R,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

: 1226764-18-6
(23S,25S)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

: 1226764-20-0
(23S,25R)-2α-methyl-1α,25-dihydroxyvitamin D3-26,23-lactam-N-(2-phenethyl)

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 18 h / 20 °C / Inert atmosphere

2: triethylamine / triphenylphosphine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex / toluene / 2 h / 120 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 50 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; triethylamine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene;