2-(3-{[5-(4-Methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]amino}phenyl)acetic hydrazide

Base Information

Chemical Name:2-(3-{[5-(4-Methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]amino}phenyl)acetic hydrazide
CAS No.:943344-70-5
Molecular Formula:C₂₇H₂₃N₅O₃
Molecular Weight:465.511
Hs Code.:

Synonyms:2-(3-{[5-(4-Methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]amino}phenyl)acetic hydrazide

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Chemical Property of 2-(3-{[5-(4-Methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]amino}phenyl)acetic hydrazide

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Technology Process of 2-(3-{[5-(4-Methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]amino}phenyl)acetic hydrazide

There total 5 articles about 2-(3-{[5-(4-Methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]amino}phenyl)acetic hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.3%

: 943344-71-6
3-{[5-(4-methoxy-phenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]amino}phenylacetic acid methyl ester

: 943344-70-5
2-(3-{[5-(4-Methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]amino}phenyl)acetic hydrazide

Guidance literature:: With hydrazine hydrate; In tetrahydrofuran; methanol; at 20 - 65 ℃;

Reference yield:

: 4254-17-5
4-methoxybenzoin

: 943344-70-5
2-(3-{[5-(4-Methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]amino}phenyl)acetic hydrazide

Guidance literature:: Multi-step reaction with 5 steps

1.1: diethylamine / N,N-dimethyl-formamide / 5 h / 20 °C / Cooling with ice

2.1: acetic anhydride / 0 °C

2.2: 10 - 130 °C

3.1: trichlorophosphate / 1 h / Reflux

3.2: 55 - 75 °C / pH 9

4.1: 1.5 h / 150 °C

5.1: hydrazine hydrate / tetrahydrofuran; methanol / 20 - 65 °C

With acetic anhydride; hydrazine hydrate; diethylamine; trichlorophosphate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 14774-62-0
2-amino-4-(4-methoxyphenyl)-5-phenylfuran-3-carbonitrile

: 943344-70-5
2-(3-{[5-(4-Methoxyphenyl)-6-phenylfuro[2,3-d]pyrimidin-4-yl]amino}phenyl)acetic hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic anhydride / 0 °C

1.2: 10 - 130 °C

2.1: trichlorophosphate / 1 h / Reflux

2.2: 55 - 75 °C / pH 9

3.1: 1.5 h / 150 °C

4.1: hydrazine hydrate / tetrahydrofuran; methanol / 20 - 65 °C

With acetic anhydride; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; methanol;