(2-chlorophenyl)-(3-mercapto-5-oxopiperidin-1-yl)acetic acid methyl ester

Base Information

Chemical Name:(2-chlorophenyl)-(3-mercapto-5-oxopiperidin-1-yl)acetic acid methyl ester
CAS No.:1373492-33-1
Molecular Formula:C₁₄H₁₆ClNO₃S
Molecular Weight:313.805
Hs Code.:

Synonyms:(2-chlorophenyl)-(3-mercapto-5-oxopiperidin-1-yl)acetic acid methyl ester

Suppliers and Price of (2-chlorophenyl)-(3-mercapto-5-oxopiperidin-1-yl)acetic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2-chlorophenyl)-(3-mercapto-5-oxopiperidin-1-yl)acetic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2-chlorophenyl)-(3-mercapto-5-oxopiperidin-1-yl)acetic acid methyl ester

There total 6 articles about (2-chlorophenyl)-(3-mercapto-5-oxopiperidin-1-yl)acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373492-32-0
(2-chlorophenyl)-(3-oxo-3,6-dihydro-2H-pyridin-1-yl)acetic acid methyl ester

: 1373492-33-1
(2-chlorophenyl)-(3-mercapto-5-oxopiperidin-1-yl)acetic acid methyl ester

Guidance literature:: With hydrogen sulfide; triethylamine; In methanol; for 1.25h; Inert atmosphere;

Reference yield:

: 120568-74-3
N-allyl-N-(2-hydroxy-3-butenyl)amine

: 1373492-33-1
(2-chlorophenyl)-(3-mercapto-5-oxopiperidin-1-yl)acetic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / 1,4-dioxane; water / 20 °C / Cooling in water bath

2: Grubbs catalyst first generation / dichloromethane / 20 °C / Inert atmosphere

3: pyridinium chlorochromate / dichloromethane / 1 h / Inert atmosphere

4: dichloromethane / 4 h / 20 °C / Inert atmosphere

5: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

6: triethylamine; hydrogen sulfide / methanol / 1.25 h / Inert atmosphere

With hydrogen sulfide; potassium carbonate; triethylamine; pyridinium chlorochromate; sodium hydroxide; Grubbs catalyst first generation; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: allyl-(1-hydroxyallyl)carbamic acid tert-butyl ester

: 1373492-33-1
(2-chlorophenyl)-(3-mercapto-5-oxopiperidin-1-yl)acetic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: Grubbs catalyst first generation / dichloromethane / 20 °C / Inert atmosphere

2: pyridinium chlorochromate / dichloromethane / 1 h / Inert atmosphere

3: dichloromethane / 4 h / 20 °C / Inert atmosphere

4: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

5: triethylamine; hydrogen sulfide / methanol / 1.25 h / Inert atmosphere

With hydrogen sulfide; potassium carbonate; triethylamine; pyridinium chlorochromate; Grubbs catalyst first generation; In methanol; dichloromethane; N,N-dimethyl-formamide;