N-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-4-([2,2';6',2'']terpyridin-4'-yloxy)-butyramide

Base Information

Chemical Name:N-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-4-([2,2';6',2'']terpyridin-4'-yloxy)-butyramide
CAS No.:913081-77-3
Molecular Formula:C₄₃H₄₂N₄O₆
Molecular Weight:710.83
Hs Code.:

<i>N</i>-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-4-([2,2';6',2'']terpyridin-4'-yloxy)-butyramide

Synonyms:N-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-4-([2,2';6',2'']terpyridin-4'-yloxy)-butyramide

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Chemical Property of N-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-4-([2,2';6',2'']terpyridin-4'-yloxy)-butyramide

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Technology Process of N-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-4-([2,2';6',2'']terpyridin-4'-yloxy)-butyramide

There total 2 articles about N-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-4-([2,2';6',2'']terpyridin-4'-yloxy)-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 168642-00-0
4-<4'-Oxa-(2,2':6',2''-terpyridinyl)>butanoic acid

: 213550-25-5
(R)-3-DMTr-serinol

: 913081-77-3
N-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-4-([2,2';6',2'']terpyridin-4'-yloxy)-butyramide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1080/15257770500230426

Reference yield:

: 913081-76-2
(S)-3-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-(2,2,2-trifluoro-acetylamino)-propionic acid ethyl ester

: 913081-77-3
N-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-hydroxymethyl-ethyl}-4-([2,2';6',2'']terpyridin-4'-yloxy)-butyramide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium borohydride; lithium chloride / ethanol / 12 h / 0 - 20 °C

2: 60 percent / EDC-HCl; 1-hydroxybenzotriazole / dimethylformamide / 12 h / 20 °C

With sodium tetrahydroborate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium chloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/15257770500230426