Technology Process of C51H39N3O
There total 10 articles about C51H39N3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium fluoride;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
N,N-dimethyl-formamide;
at 80 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium(0) / toluene; hexanes / 120 °C / Inert atmosphere
2.1: boron tribromide / dichloromethane / -77 - 20 °C / Inert atmosphere
2.2: 0.75 h
3.1: caesium carbonate / copper(l) iodide / 1,4-dioxane / 120 °C / Inert atmosphere
4.1: potassium fluoride / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
With
potassium fluoride; boron tribromide; caesium carbonate; sodium t-butanolate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium(0); copper(l) iodide; tri-tert-butyl phosphine;
In
1,4-dioxane; hexanes; dichloromethane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 20 °C
2: trichlorophosphate / 1,4-dioxane / 100 °C
3: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 80 °C / Inert atmosphere
4: potassium fluoride / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
With
potassium fluoride; potassium acetate; triethylamine; trichlorophosphate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;