bis(2-methylphenyl)iodonium trifluoromethanesulfonic acid

Base Information

Chemical Name:bis(2-methylphenyl)iodonium trifluoromethanesulfonic acid
CAS No.:1374643-16-9
Molecular Formula:CF₃O₃S*C₁₄H₁₄I
Molecular Weight:458.24
Hs Code.:

Synonyms:bis(2-methylphenyl)iodonium trifluoromethanesulfonic acid

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Chemical Property of bis(2-methylphenyl)iodonium trifluoromethanesulfonic acid

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Technology Process of bis(2-methylphenyl)iodonium trifluoromethanesulfonic acid

There total 3 articles about bis(2-methylphenyl)iodonium trifluoromethanesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 615-37-2
ortho-methylphenyl iodide

: 1493-13-6
trifluorormethanesulfonic acid

: 16419-60-6
2-Methylphenylboronic acid

: 1374643-16-9
bis(2-methylphenyl)iodonium trifluoromethanesulfonic acid

Guidance literature:: ortho-methylphenyl iodide; With boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

2-Methylphenylboronic acid; In dichloromethane; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1002/chem.201102770

Reference yield:

: 1493-13-6
trifluorormethanesulfonic acid

: 31599-59-4
2-(diacetoxyiodo)toluene

: 16419-60-6
2-Methylphenylboronic acid

: 1374643-16-9
bis(2-methylphenyl)iodonium trifluoromethanesulfonic acid

Guidance literature:: 2-Methylphenylboronic acid; With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 0.166667h;

2-(diacetoxyiodo)toluene; In dichloromethane; at 0 - 20 ℃; for 1.16667h;

trifluorormethanesulfonic acid; In dichloromethane; at 0 - 20 ℃; for 0.333333h;
DOI:10.1039/c7gc02844j