4,4a,5,7a-tetrahydro-3-phenyl-5-(trimethylsilyl)cyclopent-1,2-oxazine

Base Information

Chemical Name:4,4a,5,7a-tetrahydro-3-phenyl-5-(trimethylsilyl)cyclopent-1,2-oxazine
CAS No.:124462-62-0
Molecular Formula:C₁₆H₂₁NOSi
Molecular Weight:271.434
Hs Code.:

4,4a,5,7a-tetrahydro-3-phenyl-5-(trimethylsilyl)cyclopent<e>-1,2-oxazine

Synonyms:4,4a,5,7a-tetrahydro-3-phenyl-5-(trimethylsilyl)cyclopent-1,2-oxazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4a,5,7a-tetrahydro-3-phenyl-5-(trimethylsilyl)cyclopent-1,2-oxazine

Chemical Property:

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Technology Process of 4,4a,5,7a-tetrahydro-3-phenyl-5-(trimethylsilyl)cyclopent-1,2-oxazine

There total 1 articles about 4,4a,5,7a-tetrahydro-3-phenyl-5-(trimethylsilyl)cyclopent-1,2-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3559-74-8
trimethylsilylcyclopentadiene

: 21572-32-7
2-chloro-1-phenyl-ethanone oxime

: 124462-62-0
4,4a,5,7a-tetrahydro-3-phenyl-5-(trimethylsilyl)cyclopent-1,2-oxazine

Guidance literature:: With sodium carbonate; In diethyl ether; for 72h; Ambient temperature;

Reference yield:

: 124462-62-0
4,4a,5,7a-tetrahydro-3-phenyl-5-(trimethylsilyl)cyclopent-1,2-oxazine

: 128710-07-6
C₁₆H₂₀⁽²⁾HNOSi

: 128779-05-5
C₁₆H₂₀⁽²⁾HNOSi

Guidance literature:: With n-butyllithium; water-d2; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1) THF, -78 deg C, 15 min, 2) -78 deg C, 1 h;