(S)-6-((3-(2-methylamino)propyl)phenoxy)-N-(2-(tritylthio)ethyl)hexanamide

Base Information

Chemical Name:(S)-6-((3-(2-methylamino)propyl)phenoxy)-N-(2-(tritylthio)ethyl)hexanamide
CAS No.:1313762-89-8
Molecular Formula:C₃₇H₄₄N₂O₂S
Molecular Weight:580.835
Hs Code.:

Synonyms:(S)-6-((3-(2-methylamino)propyl)phenoxy)-N-(2-(tritylthio)ethyl)hexanamide

Suppliers and Price of (S)-6-((3-(2-methylamino)propyl)phenoxy)-N-(2-(tritylthio)ethyl)hexanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-6-((3-(2-methylamino)propyl)phenoxy)-N-(2-(tritylthio)ethyl)hexanamide

Chemical Property:

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Technology Process of (S)-6-((3-(2-methylamino)propyl)phenoxy)-N-(2-(tritylthio)ethyl)hexanamide

There total 8 articles about (S)-6-((3-(2-methylamino)propyl)phenoxy)-N-(2-(tritylthio)ethyl)hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1338381-55-7
C₄₂H₅₂N₂O₄S

: 1313762-89-8
(S)-6-((3-(2-methylamino)propyl)phenoxy)-N-(2-(tritylthio)ethyl)hexanamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1021/jm2004943

Reference yield:

: 1095-85-8
2-amino tritylthio ethane

: 1313762-88-7
(S)-6-(3-(2-(tert-butoxycarbonyl(methyl)amino)propyl)phenoxy)hexanoic acid

: 1313762-89-8
(S)-6-((3-(2-methylamino)propyl)phenoxy)-N-(2-(tritylthio)ethyl)hexanamide

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm2004943

Reference yield:

: 1313762-85-4
(S)-3-(2-(methylamino)propyl)phenol hydrobromide

: 1313762-89-8
(S)-6-((3-(2-methylamino)propyl)phenoxy)-N-(2-(tritylthio)ethyl)hexanamide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / methanol / 0.5 h / Reflux

2: sodium hydride / hexanes; N,N-dimethyl-formamide / 16 h

3: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 8 h / Reflux

4: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; water; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; hexanes; N,N-dimethyl-formamide;
DOI:10.1021/jm2004943